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A Chemometrics Approach Comparing Volatile Changes during the Shelf Life of Apple Juice Processed by Pulsed Electric Fields High Pressure and Thermal Pasteurization

机译:化学计量学方法比较通过脉冲电场高压和热巴氏杀菌处理的苹果汁保质期内的挥发性变化

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摘要

High-Pressure Processing (HPP) and Pulsed Electric Fields (PEF) processing technologies are being used increasingly on a commercial basis, with high-quality labelled fruit juices being one of the most important promotion strategies. Quality-related enzymes, which might still be active after HPP and PEF pasteurization, can cause undesirable aroma changes during storage. This study investigated volatile changes during the shelf life of PEF (15.5 kV/cm and specific energy of 158 kJ/L), HPP (600 MPa for 3 min), and thermally (72 °C for 15 s) pasteurized Jazz apple juices—up to five weeks. To have an increased insight into the volatile changes, an integrated instrumental (GC-MS) and data analysis (chemometrics) approach was implemented. Immediately after pasteurization, PEF processing resulted a better retention of odor-active volatiles, such as (E)-2-hexenal and hexyl acetate, whereas thermal processing lowered their amount. During refrigerated storage, these volatiles have gradually decreased in all processed juices. By the end of storage, the amount of these aroma relevant volatiles appears to still be higher in PEF and HPP pasteurized juices compared to their conventional counterparts. This study demonstrated the potential of advanced chemometric approaches to obtain increased insight into complex shelf life changes.
机译:高压加工(HPP)和脉冲电场(PEF)加工技术已在商业上得到越来越多的使用,高质量的带标签果汁是最重要的推广策略之一。与质量相关的酶(在HPP和PEF巴氏消毒后仍可能具有活性)会在存储过程中引起不良的香气变化。这项研究调查了PEF(15.5 kV / cm和比能158 kJ / L),HPP(600 MPa持续3分钟)和热(72°C持续15 s)巴氏灭菌的爵士苹果汁的货架期中的挥发性变化-最多五个星期。为了增加对波动变化的了解,已实施了集成的仪器(GC-MS)和数据分析(化学计量学)方法。巴氏灭菌后立即进行PEF处理,从而更好地保留了具有气味活性的挥发性物质,例如(E)-2-己烯醛和乙酸己酯,而热处理降低了其含量。在冷藏过程中,所有加工果汁中的这些挥发物已逐渐减少。到存储结束时,PEF和HPP巴氏杀菌果汁中与传统香精相比,这些与香气有关的挥发物的数量似乎仍然更高。这项研究证明了先进的化学计量学方法可能获得对复杂货架寿命变化的更多了解。

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