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A survey of the incidence and level of aflatoxin contamination in a range of imported spice preparations on the Irish retail market

机译:爱尔兰零售市场上一系列进口香料制剂中黄曲霉毒素污染的发生率和水平的调查

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摘要

The aflatoxin contents of 130 commercial spice preparations, including pepper, chilli, curry powder, cayenne, paprika, cinnamon, coriander, turmeric and cumin, were determined using high performance liquid chromatography (HPLC). Samples were obtained from various retail outlets in Ireland, including supermarkets, shops and market stalls. Aflatoxin B1 gave the highest incidence of contamination in spice preparations and was found in 20 of the 130 samples. The highest concentration of aflatoxin, 27.5 μg/kg, was detected in a sample of chilli powder; next highest was in a sample of cayenne pepper which contained 18.5 μg/kg. Five samples (3.8%), consisting of chilli, cayenne pepper and turmeric pepper, were above the regulatory limits of the European Union. Aflatoxin contamination was not detected in cumin or cinnamon samples at a level of quantitation (LOQ) <0.2, <0.1, <0.5, <0.3 μg/kg for B1, B2, G1 and G2, respectively.
机译:使用高效液相色谱(HPLC)测定了130种市售香料制剂中的黄曲霉毒素含量,包括胡椒,辣椒,咖喱粉,辣椒,辣椒粉,肉桂,香菜,姜黄和小茴香。样品是从爱尔兰的各种零售商店(包括超市,商店和市场摊位)获得的。黄曲霉毒素B1在香料制剂中污染的发生率最高,在130个样品中有20个被发现。在辣椒粉样品中,黄曲霉毒素的最高浓度为27.5μg/ kg。第二高的是辣椒样品,含量为18.5μg/ kg。五个样本(3.8%)由辣椒,辣椒和姜黄胡椒组成,超过了欧盟的监管规定。在小茴香或肉桂样品中,B1,B2,G1和G2的定量(LOQ)分别<0.2,<0.1,<0.5,<0.3μg/ kg,未检出黄曲霉毒素污染。

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