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Study on Damping Property of Epoxy-Matrix with PbZr_(0.47)Ti_(0.53)O_3 Piezoelectric Film Effect

机译:PbZr_(0.47)Ti_(0.53)O_3压电薄膜效应对环氧树脂基体阻尼性能的影响

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A new type of rigid piezo-damping epoxy-matrix composites containing piezoelectric lead zirconate titanate thin films was prepared. The PbZr_(0.47)Ti_(0.53)O_3 thin films were fabricated on the Pt/Ti/SiO_2/Si substrates by sol-gel method. The crystal structure of the films was characterized. The thin films showed a perovskite phase by changing annealing temperature. The produced film and the substrates have been joined into epoxy resin as constrained layer, and then the damping property of composites has been study. Through improving the annealing process when proparing film, the optimum filming technology which can improve the damping property of composites has obtained. The film was hatedup to 700°C with 10°C/min and holding time for 30min, then cooling with furnace. By this way, The dielectric constant and the dissipation factor of the PbZr_(0.47)Ti_(0.53)O_3 thin films were about 480 and 0.027 at 1MHz, respectively.The peak of the damping tan8 has reached 0.923. The results show that when the Pb(Zr_(0.53)Ti_(0.47))O_3 thin films annealed at 700°C, the damping loss factor of the composites has reached the maximum.
机译:制备了一种新型的含有压电锆钛酸铅钛酸酯薄膜的刚性压电阻尼环氧基复合材料。采用溶胶-凝胶法在Pt / Ti / SiO_2 / Si衬底上制备了PbZr_(0.47)Ti_(0.53)O_3薄膜。表征膜的晶体结构。通过改变退火温度,薄膜显示出钙钛矿相。将制得的薄膜和基材作为约束层结合到环氧树脂中,然后研究了复合材料的阻尼性能。通过改进薄膜成膜时的退火工艺,获得了可以改善复合材料阻尼性能的最佳成膜技术。这部电影令人讨厌 以10°C / min的速度升至700°C,并保持30分钟,然后用炉子冷却。这样,PbZr_(0.47)Ti_(0.53)O_3薄膜的介电常数和耗散因数在1MHz时分别约为480和0.027,阻尼tan8的峰值已达到0.923。结果表明,当Pb(Zr_(0.53)Ti_(0.47))O_3薄膜在700°C退火时,复合材料的阻尼损耗因子达到最大值。

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