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Study of the fatty acid profile and the aroma composition of oil obtained from roasted Colombian coffee beans by supercritical fluid extraction

机译:超临界流体萃取从哥伦比亚烘培咖啡豆中提取的油的脂肪酸组成和香气成分的研究

摘要

In the present work, the extraction of oil from roasted coffee beans using supercritical carbon dioxide (CO) under different conditions of pressure (15-30 MPa) and temperature (40-60°C) was studied. A central composite experimental design was employed in order to establish the effect of these parameters on the yield and fatty acids composition that was determined by gas chromatography with flame ionization detector (GC-FID). The aroma was analyzed by headspace solid phase microextraction (HS-SPME). The optimum oil yield was 8.9%, obtained at 33.1 MPa and 35.9°C. The main fatty acids identified were palmitic (46.1%), linoleic (32.9%), oleic (8.0%), stearic (6.6%) and arachidic (1.9%). The volatile compounds of the coffee oil belong mainly to the family of furans and pyrazines, which maintain the particular features of the roasted coffee. This fact makes the coffee oil attractive to be used in the food and/or cosmetic industry.
机译:在当前工作中,研究了在不同压力(15-30 MPa)和温度(40-60°C)条件下使用超临界二氧化碳(CO)从烘焙咖啡豆中提取油的方法。为了确定这些参数对产率和脂肪酸组成的影响,采用了中央复合实验设计,通过气相色谱和火焰离子化检测器(GC-FID)确定了这些参数。通过顶空固相微萃取(HS-SPME)分析香气。最佳油产率为8.9%,在33.1 MPa和35.9°C下获得。确定的主要脂肪酸为棕榈酸(46.1%),亚油酸(32.9%),油酸(8.0%),硬脂酸(6.6%)和花生酸(1.9%)。咖啡油的挥发性化合物主要属于呋喃和吡嗪类,它们保持了焙炒咖啡的特殊功能。这个事实使咖啡油具有吸引力,可用于食品和/或化妆品工业。

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