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Ultrasound-assisted Extraction and Characterizations of Pectins from Dragon Fruit (Hylocereus polyrhizus) Peels in Various Acid Solution: A Preliminary Study

机译:超声在多种酸溶液中提取火龙果果皮中果胶的初步研究

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摘要

The worldwide consumption of pectin was reported about 45 million kilogram per annum. Due to some major demand of pectin in food and pharmaceutical industries, numerous investigations have been carried out to determine the composition of pectin in different plant. A major challenge in developing any new pectin product is to preserve the physicochemical characteristics of pectin. This is due to composition of pectin can vary depending on the plant source and extraction condition. This study was focused on the potential of Hylocereus polyrhizus peels (HPP) to be a source of pectin. The extraction of pectin from HPP was carried out using combine method of physical and chemical during extraction. The equipment used was sonicator bath attach with propeller stirrer and extraction was carried out in dionized water, organic acid (citric acid, acetic acid) and mineral acid (H2SO4, HCl, HNO3). Pectin obtain from this method was compared in terms of yield, galacturonic acid (GalA) content and degree of esterification (DE). Fourier Transform Infrared Spectroscopy (FTIR) and Ultra Violet-visible spectroscopy (UV-vis) was used in the identification of HPP pectin properties. The yield of HPP pectin range obtained was from 33% to 40% with the GalA content from 22% to 40% and DE from 13% to 62%. The highest pectin yield (~40%) with GalA 39% and DE 62% can be achieved when extraction was carried out using citric acid solution. These results suggest that ultrasound-assisted extraction could be a good option for the pectin extraction with citric acid from HPP for industrial scale.
机译:据报道,全世界果胶的消费量约为每年4500万公斤。由于食品和制药工业中果胶的一些主要需求,已经进行了许多研究以确定不同植物中果胶的组成。开发任何新的果胶产品的主要挑战是保持果胶的理化特性。这是由于果胶的成分可根据植物来源和提取条件而变化。这项研究的重点是猪齿豆(Hylocereus polyrhizus)果皮(HPP)成为果胶来源的潜力。 HPP中果胶的提取是在提取过程中采用物理和化学结合的方法进行的。所用的设备是带有螺旋桨式搅拌器的超声浴锅,并在去离子水,有机酸(柠檬酸,乙酸)和无机酸(H2SO4,HCl,HNO3)中进行萃取。比较从该方法获得的果胶的产率,半乳糖醛酸(GalA)含量和酯化度(DE)。傅里叶变换红外光谱(FTIR)和紫外可见光谱(UV-vis)用于鉴定HPP果胶特性。获得的HPP果胶范围的产率为33%至40%,GalA含量为22%至40%,DE为13%至62%。当使用柠檬酸溶液进行萃取时,使用GalA 39%和DE 62%可获得最高的果胶收率(〜40%)。这些结果表明,超声辅助提取对于从工业规模的HPP柠檬酸中提取果胶是一个很好的选择。

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