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Effect of the ways of adding stearic acid on properties of sweet potato starch and sweet-potato-starch-based films

机译:硬脂酸添加方式对甘薯淀粉和甘薯淀粉基膜性能的影响

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摘要

Starch-fatty acid composites were prepared using sweet potato starch (SPS) and stearic acid (SA). The SA was added into the starch system by employing two different ways; i.e., either prior to heating (Method I) or after heating (Method II). The ways of adding SA changed the SPS pasting characteristics as determined by Rapid Viscosity Analyzer (RVA). In differential scanning calorimetry (DSC) thermograms, both of the composites exhibited a new peak which was regarded as the melting peak of amylose-lipid complex. Scanning electronic microscope (SEM) images indicated that the quantity of intact starch granules decreased (Method I), while the starch granules in the composite prepared by Method II remained the intact morphology. The composite prepared by Method I exhibited lower relative crystallinity than their counterparts. Compared with the control film, the light transmission of the films prepared by Method I showed a decrease of 10.1%, while the films prepared by Method II exhibited a decrease of 5.1%. The films prepared by Method II had better moisture barrier properties than the films prepared by Method I. The films prepared by Method II showed higher tensile strength and elongation at break values compared with the films prepared by Method I.
机译:使用甘薯淀粉(SPS)和硬脂酸(SA)制备淀粉-脂肪酸复合材料。通过两种不同的方式将SA添加到淀粉系统中。即,在加热之前(方法I)或加热之后(方法II)。添加SA的方式改变了由快速粘度分析仪(RVA)确定的SPS粘贴特性。在差示扫描量热法(DSC)的热分析图中,两种复合物均显示出新的峰,该峰被视为直链淀粉-脂质复合物的熔融峰。扫描电子显微镜(SEM)图像表明,完整淀粉颗粒的数量减少了(方法I),而用方法II制备的复合材料中的淀粉颗粒保持了完整的形态。用方法Ⅰ制得的复合材料的相对结晶度低于其相应的结晶度。与对照膜相比,通过方法I制备的膜的透光率降低了10.1%,而通过方法II制备的膜的透射率降低了5.1%。通过方法II制备的薄膜比通过方法I制备的薄膜具有更好的防潮性能。通过方法II制备的薄膜比通过方法I制备的薄膜具有更高的拉伸强度和断裂伸长率。

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