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Optimization of spray drying process parameters for kefir powder using response surface methodology

机译:使用响应面法优化开菲尔粉的喷雾干燥工艺参数

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In this study response surface methodology (RSM) was used to optimize the spray drying process conditions for production of kefir powder. Influence of inlet air temperature (120-180 degrees C), feed temperature (4-30 degrees C) and pump rate (20-40%) on the survival rates of microorganisms, outlet temperature, moisture content and water activity were assessed after drying and modeled by RSM. A lab-scale spray dryer (Mini Spray Dryer B-290, Switzerland) was used to carry out the drying experiments which are planned according to Central Composite Rotatable Design (CCRD). Inlet temperature was found as the main factor that effects the all responses statistically significant (p < 0.05). Effect of pump rate on the responses was found significant for some responses. Feed temperature has no significant effect for any responses. The optimum conditions were found as 135 degrees C inlet air temperature and 35% pump rate with using Desirability Function. Desired parameters were determined in regard to model fit and lack of fit test analysis results. At the end of this study, optimum conditions of spray drying were matched with freeze drying results. Results showed that at the optimum point, good quality powder can be obtained as freeze dried powder quality. (C) 2014 Elsevier Ltd. All rights reserved.
机译:在这项研究中,使用响应表面方法(RSM)来优化生产克菲尔粉的喷雾干燥工艺条件。干燥后评估进气温度(120-180摄氏度),进料温度(4-30摄氏度)和泵速(20-40%)对微生物存活率,出口温度,水分含量和水分活度的影响并由RSM建模。实验室规模的喷雾干燥器(Mini Spray Dryer B-290,瑞士)用于进行干燥实验,干燥实验是根据中央复合旋转设计(CCRD)计划的。发现进水温度是影响所有响应的主要因素,具有统计学意义(p <0.05)。对于某些响应,发现泵速对响应的影响很大。进料温度对任何响应均无明显影响。使用Desirability Function确定了最佳条件是135摄氏度的进气温度和35%的泵速。确定有关模型拟合和缺乏拟合测试分析结果的所需参数。在研究结束时,喷雾干燥的最佳条件与冷冻干燥的结果相匹配。结果表明,在最佳点,可以得到高质量的粉末作为冷冻干燥的粉末。 (C)2014 Elsevier Ltd.保留所有权利。

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