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Development of Compact SEM Equipped with Carbon Nanotube Field Emission Cathode

机译:开发紧凑型SEM,配备碳纳米管场发射阴极

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Field emission (FE) properties of carbon related materials such as carbon nanotubes, carbon nanofibers, and graphite nanoneedles are currently assessed as excellent FE cathode materials which can be operated under non-ultrahigh vacuum condition for various applications. Indeed, Matsumoto et al have reported about a cold cathode SEM with a graphite nanoneedle cathode [1]. We are developing a compact FE-SEM equipped with a multiwall carbon nanotubes (MWNTs) bundle cathode and a Butler electrostatic lens as a condenser lens. The preliminary results are reported in this paper. Figure 1 shows a schematic diagram of compact FE-SEM we developed. A MWNTs bundle produced by arc discharge in helium gas was adhered to a top of tungsten hairpin filament by a conducting paste. The Butler lens consisted of an extraction and a focusing electrode was placed in front of the MWNTs bundle cathode. A ballast resistor was connected to the extraction electrode in order to stabilize an emission current. To obtain a fine probe beam, the electron beam passing through a deflector followed by the Butler lens was focused by means of an objective lens made of a permanent magnet. The adoption of these two lenses brought about downsizing to our FE-SEM column, and a distance between the cathode and the sample stage was only 192mm.
机译:目前评估碳纳米管,碳纳米纤维和石墨纳金属如碳纳米管,碳纳米纤维和石墨纳米纳米碳的碳相关材料的场发射(Fe)性质作为优异的Fe阴极材料,其可以在非超高真空条件下进行各种应用。实际上,Matsumoto等人已经报道了具有石墨纳尼罩阴极的冷阴极SEM [1]。我们正在开发配备有多壁碳纳米管(MWNT)束阴极的紧凑型Fe-SEM和作为冷凝器透镜的Butler静电透镜。本文报道了初步结果。图1显示了我们开发的Compact Fe-SEM的示意图。通过导电浆料粘附通过氦气中的电弧放电产生的MWNT束粘附到钨毛片丝的顶部。由提取和聚焦电极组成的管夹透镜置于MWNTS束阴极的前面。压载电阻连接到提取电极以稳定发射电流。为了获得精细探针光束,通过由永磁体制成的物镜聚焦通过偏转器之后的偏转的电子束。采用这两个镜片缩小到我们的Fe-SEM柱,阴极与样品阶段之间的距离仅为192mm。

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