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Scanning transmission electron microscope equipped with an electron beam energy loss spectrometer and its observation method

机译:装有电子束能量损失谱仪的扫描透射电子显微镜及其观察方法

摘要

The object of the present invention relates to high-resolution observation of bright field STEM, dark field image STEM and EELS at a low acceleration voltage. The present invention provides a STEM detector (11, 13) and an electron beam by changing the arrangement of the sample with respect to the optical axis direction of the primary electron beam in a transmission scanning electron microscope equipped with an electron beam energy loss spectrometer (17). It relates to controlling the capture angle of the energy loss spectrometer (17). According to the present invention, it is possible to easily control the optimum scattering angle for each of the bright field STEM, dark field STEM, and EELS while suppressing the occurrence of chromatic aberration associated with the control of the capture angle.
机译:本发明的目的涉及在低加速电压下对亮场STEM,暗场图像STEM和EELS进行高分辨率观察。本发明提供了一种STEM检测器(11、13)和一种电子束,其通过在配备有电子束能量损耗光谱仪的透射扫描电子显微镜中改变样品相对于一次电子束的光轴方向的排列来实现。 17)。它涉及控制能量损失光谱仪(17)的捕获角。根据本发明,可以容易地控制明场STEM,暗场STEM和EELS中的每一个的最佳散射角,同时抑制与捕获角的控制相关的色差的发生。

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