首页> 外国专利> ONE-STAGE METHOD FOR PRODUCTION OF HTP (HIGH TEST PEROXIDE) HYDROGEN PEROXIDE FOR PROPULSION APPLICATIONS AND SYSTEM FOR PRODUCTION THEREOF

ONE-STAGE METHOD FOR PRODUCTION OF HTP (HIGH TEST PEROXIDE) HYDROGEN PEROXIDE FOR PROPULSION APPLICATIONS AND SYSTEM FOR PRODUCTION THEREOF

机译:用于推进应用的生产过氧化氢(HTP)的一阶段方法及其生产系统

摘要

The invention relates to a one-stage system for concentration and purification of concentrated hydrogen peroxide, in particular for production of concentrated solution of HTP (High Test Peroxide) grade hydrogen peroxide of concentration of at least 98% for propulsion applications, comprising heating means, a water bath, a rotating flask with a drive in a sloping position at an angle from 105° to 140° with respect to the fractionating column, a condenser, a distillate receiver, characterised in that it additionally comprises a stationary flask (4) placed between the fractionating column (7) and the rotating flask (3) for placing the feedstock, and above the fractionating column (7) and before the condenser (10) it comprises a condenser controlled by the flow rate of the cooling liquid (8), and further behind the condenser (10) and before the stopcock (11) shutting off the main receiver (12) it comprises an auxiliary condenser (13) that from one side is connected to vacuum, and from the other side it is connected to an auxiliary receiver (15), whereas the fractionating column is an adiabatic fractionating column (7), and the final product is received from the flasks (3) and (4). Additionally, the invention comprises a method for production of concentrated solution of hydrogen peroxide, in particular of HTP (High Test Peroxide) grade of concentration of at least 98% for propulsion applications, in a system according to the invention, in which the one-stage process of production of concentrated hydrogen peroxide solution by concentration and purification of hydrogen peroxide solution is carried out.
机译:本发明涉及一种用于浓缩和纯化浓过氧化氢的一级系统,特别是用于生产浓度至少为98%的HTP(高测试过氧化物)级过氧化氢浓溶液用于推进应用,该系统包括加热装置,水浴,旋转式烧瓶,其驱动器相对于分馏塔处于倾斜位置,且倾斜角度为105°至140°,冷凝器,馏出液接收器,其特征在于,它还包括一个放置在其中的固定烧瓶(4)在分馏塔(7)和用于放置原料的旋转烧瓶(3)之间,并且在分馏塔(7)上方并且在冷凝器(10)之前,其包括由冷却液(8)的流量控制的冷凝器。 ,并且在冷凝器(10)的后面,并且在旋塞(11)关闭主接收器(12)之前,它包括一个辅助冷凝器(13),该辅助冷凝器从一侧连接到真空,从另一侧连接到真空。另一侧与辅助接收器(15)连接,而分馏塔为绝热分馏塔(7),最终产品从烧瓶(3)和(4)接收。另外,本发明包括一种在根据本发明的系统中生产浓度为至少98%的过氧化氢,特别是HTP(高测试过氧化物)浓度的推进溶液的方法,以用于推进应用。进行通过浓缩和纯化过氧化氢溶液生产浓过氧化氢溶液的阶段过程。

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