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HTP 1 One-stage method for production of HTP High Test Peroxide hydrogen peroxide for propulsion applications and system for production thereof

机译:HTP 1生产用于推进应用的HTP高压过氧化氢的一阶段方法及其生产系统

摘要

The present invention relates to a concentrating and purifying concentrate of hydrogen peroxide comprising a rotating flask with a drive at an inclined position at an angle of 105 ° to 140 ° with respect to the condenser, the distillation receiver, the fractionation column, the heating means, A system for the preparation of a HTP (High Test Peroxide) grade hydrogen peroxide concentrate at a concentration of at least 98% with respect to a propulsion application, said system comprising, for placing a feedstock, said distillation column (7) And a fixed flask (4) positioned between the fixed flask (4); The system further comprises a condenser (8) controlled by the flow rate of the cooling liquid before the top of the fractionation tower (7) and before the condenser (10); The system further includes an auxiliary capacitor 13 to which a vacuum is connected on one side and an auxiliary receiver 15 is connected on the other side before the condenser 10 and the stopper 11 for blocking the main receiver 12 ; Stage system of concentration and purification of concentrated hydrogen peroxide characterized in that said fractionation column is an adiabatic fractionation column (7) and the end product is obtained from said rotary flask (3) and said stationary flask (4) . In addition, in the system according to the present invention, a one-step process for preparing a concentrated hydrogen peroxide solution by concentration and purification of a hydrogen peroxide solution is carried out, and a high test peroxide (HTP) concentration of at least 98% 0.0 hydrogen peroxide / RTI
机译:本发明涉及一种过氧化氢的浓缩提纯浓缩物,其包括旋转烧瓶,该旋转烧瓶的驱动器相对于冷凝器,蒸馏接收器,分馏塔,加热装置以相对于冷凝器成105°至140°的角度倾斜。相对于推进应用以至少98%的浓度制备HTP(高测试过氧化物)级过氧化氢浓缩物的系统,所述系统包括用于放置原料的所述蒸馏塔(7)和位于固定烧瓶(4)之间的固定烧瓶(4);该系统还包括冷凝器(8),其由分馏塔(7)的顶部之前和冷凝器(10)之前的冷却液的流速控制;该系统还包括辅助电容器13,在冷凝器10和塞子11之前,辅助电容器13的一侧连接有真空,而辅助接收器15的另一侧连接有辅助电容器13,以阻塞主接收器12。浓缩和纯化浓过氧化氢的阶段系统,其特征在于,所述分馏塔为绝热分馏塔(7),并且从所述旋转烧瓶(3)和所述固定烧瓶(4)获得最终产物。另外,在根据本发明的系统中,进行通过浓缩和纯化过氧化氢溶液来制备浓过氧化氢溶液的一步法,并且高测试过氧化物(HTP)浓度至少为98。 %0.0>过氧化氢

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