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Challenges in quantitative analysis of aroma compounds in cheeses with different fat content and maturity level

机译:脂肪含量和成熟度不同的奶酪中的香气化合物定量分析面临的挑战

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摘要

Quantification of 62 aroma compounds in three commercial semi-hard cheeses with different fat contents and maturity levels was pursued. Dynamic headspace sampling and gas chromatography-mass spectrometry (GC-MS) was applied after spiking each of the three cheeses with the aroma compounds, and PARAllel FACtor analysis was used to resolve co-eluting compounds. By the use of linear regression, half of the spiked aroma compounds exhibited similar slopes in the three cheeses whereas the volatilities of 15 other compounds were dependent on their hydrophilicity relative to the fat content of the cheese. For nine aroma compounds, satisfactory coefficients of determination were obtained in one or two of the cheeses only, and seven compounds could not be quantified at all.
机译:对三种脂肪含量和成熟度不同的商用半硬奶酪中的62种香气化合物进行了定量分析。在将三种干酪中的每一种都加入芳香化合物后,采用动态顶空进样和气相色谱-质谱联用(GC-MS),并使用PARAllel FACtor分析法来分离共洗脱化合物。通过线性回归,在三种奶酪中加标的芳香化合物中有一半的斜率相似,而其他15种化合物的挥发性取决于它们相对于奶酪脂肪含量的亲水性。对于9种香气化合物,仅在一种或两种干酪中获得了令人满意的测定系数,而根本无法对7种化合物进行定量。

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