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首页> 外文期刊>Journal of separation science. >Analysis of tetracyclines from milk powder by molecularly imprinted solid‐phase dispersion based on a metal–organic framework followed by ultra high performance liquid chromatography with tandem mass spectrometry
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Analysis of tetracyclines from milk powder by molecularly imprinted solid‐phase dispersion based on a metal–organic framework followed by ultra high performance liquid chromatography with tandem mass spectrometry

机译：基于金属 - 有机框架的分子印迹固相分散的奶粉中四环素分析，用串联质谱法进行超高效液相色谱法

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Abstract > A novel molecularly imprinted polymer that could selectively recognize tetracyclines in milk powder was synthesized using a metal–organic framework as a support material, tetracycline as template molecule, and 3‐aminophenylboronic acid as a functional monomer and a cross‐linking agent. The novel molecularly imprinted polymer was characterized by Fourier transform infrared spectrometry, transmission electron microscopy, X‐ray diffractometry, thermogravimetric analysis, and N <sub>2</sub> adsorption/desorption measurements. The adsorption isotherms, adsorption kinetics, adsorption thermodynamics, and selective adsorption experiments of the novel molecularly imprinted polymer to tetracycline were also studied. The novel molecularly imprinted polymer was used as dispersant of matrix solid‐phase dispersion to extraction tetracyclines. After that, the tetracyclines extracted from milk powder were determined by ultra high performance liquid chromatography with tandem mass spectrometry. Under the optimal conditions, the detection limits of tetracyclines were 0.217–0.318?ng/g. The relative standard deviations of intra‐ and interday precision ranged from 3.8 to 6.9% and from 2.8 to 7.4%, respectively. In all three concentration levels (1.0, 10, 50?ng/g), the recoveries of tetracyclines ranged from 84.7 to 93.9%. The method was successfully applied to the determination of tetracyclines in milk powder. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“En”> <标题类型=“main”>摘要</标题> >可以使用金属选择性地识别奶粉中四环素的新型分子印迹聚合物。作为载体材料，四环素作为模板分子和3-氨基苯基硼酸作为官能单体和交联剂的有机框架。通过傅里叶变换红外光谱法，透射电子显微镜，X射线衍射测定法，热重分析和N <亚> 2 </ Sub>吸附/解吸测量，表征了新的分子印迹聚合物。还研究了吸附等温线，吸附动力学，吸附热力学以及新型分子印迹聚合物对四环素的选择性吸附试验。该新型分子印迹聚合物用作基质固相分散体的分散剂，以提取四环素。之后，通过用串联质谱法通过超高化性液相色谱法测定从牛奶粉末中提取的四环素。在最佳条件下，四环素的检测限为0.217-0.318≤ng/ g。内部和中间精度的相对标准偏差分别为3.8％至6.9％，分别为2.8％至7.4％。在所有三种浓度水平（1.0,10,50？Ng / g）中，四环素的回收率范围为84.7％至93.9％。该方法成功地应用于奶粉中四环素的测定。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2018年第12期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Shangshu&option=202" target="_blank" rel="nofollow">Wang Shangshu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Jianfeng&option=202" target="_blank" rel="nofollow">Zhang Jianfeng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Chenyu&option=202" target="_blank" rel="nofollow">Li Chenyu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Ligang&option=202" target="_blank" rel="nofollow">Chen Ligang;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of ChemistryNortheast Forestry UniversityHarbin China;</p> <p>Center of Disease Control of Heilongjiang ProvinceHarbin China;</p> <p>Center of Disease Control of Heilongjiang ProvinceHarbin China;</p> <p>Department of ChemistryNortheast Forestry UniversityHarbin China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=matrix solid‐phase dispersion&option=203" rel="nofollow">matrix solid‐phase dispersion;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=metal–organic frameworks&option=203" rel="nofollow">metal–organic frameworks;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=milk powder&option=203" rel="nofollow">milk powder;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=molecularly imprinted polymers&option=203" rel="nofollow">molecularly imprinted polymers;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=tetracyclines&option=203" rel="nofollow">tetracyclines;</a> </p> <div class="translation"> 机译：基质固相分散;金属 - 有机框架;奶粉;分子印迹聚合物;四环素; 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