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首页> 外文期刊>Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics >In situ synthesis and photoluminescence of SiC nanowires by microwave-assisted pyrolysis of methane
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In situ synthesis and photoluminescence of SiC nanowires by microwave-assisted pyrolysis of methane

机译:微波辅助甲烷热解原位合成SiC纳米线及其光致发光

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A simple method was used to synthesize SiC nanowires directly on quartz plate by microwave pyrolysis of methane. The samples have been characterized by field emission scanning electron microscopy, transmission electron microscopy, X-ray diffraction and Raman spectroscopy techniques. The results showed that the nanowires are of cubic beta-SiC structure with stacking faults. The diameters of SiC nanowires are in the range of 50-200 nm and their lengths up to several tens of microns. The effect of the reaction gas concentration and the reaction temperature on the morphologies of SiC nanowires was also investigated. Two broad photoluminescence peaks at the center wavelength of about 309 and 417 nm were observed at room temperature.
机译:一种简单的方法是通过甲烷的微波热解直接在石英板上合成SiC纳米线。通过场发射扫描电子显微镜,透射电子显微镜,X射线衍射和拉曼光谱技术对样品进行了表征。结果表明,纳米线为立方β-SiC结构,具有堆垛层错。 SiC纳米线的直径在50-200 nm的范围内,其长度可达数十微米。还研究了反应气体浓度和反应温度对SiC纳米线形貌的影响。在室温下,在中心波长约309和417 nm处观察到两个宽的光致发光峰。

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