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Study on Characteristics of Nanopowders Synthesized by Nanosecond Electrical Explosion of Thin Aluminum Wire in the Argon Gas

机译:氩气中细铝丝纳秒电爆炸合成纳米粉末的特性研究

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As a new gas-phase synthesis method for the production of nanosize powders, the wire electrical explosion method has the advantages of high energy efficiency and high product purity through production under pure inert gas conditions and has been applied to the continuous industrial production of nanopowders. In this paper, an experimental device based on the electrical explosion of metallic wires for nanopowder production and collection is designed and built. Also, aluminum nanopowders were produced by electrically exploding an aluminum wire and collected by the microporous membrane filter successfully under different pressures of argon gas. Moreover, the influence of the argon gas pressure on the characteristics of the aluminum nanopowders was analyzed by a transmission electron microscope. The results showed that the particle shape, size, and distribution of the aluminum nanopowders could be controlled by the pressure of argon gas. The aluminum nanoparticles produced in the high-pressure argon gas had better spherical particle shape; meanwhile, the count mean diameter of the aluminum nanopowders increased obviously with the rise of the argon gas pressure. A higher pressure of argon gas could broaden the range of the aluminum nanoparticle size distribution evidently.
机译:线电爆炸法是生产纳米级粉末的一种新型气相合成方法,具有在纯惰性气体条件下生产的高能效和高产品纯度的优点,已应用于纳米粉体的连续工业生产中。本文设计并建造了一种基于金属丝电爆炸的实验装置,用于纳米粉的生产和收集。另外,通过使铝线电爆炸来制造铝纳米粉末,并在不同的氩气压力下成功地通过微孔膜过滤器将其收集。此外,通过透射电子显微镜分析了氩气压力对铝纳米粉体特性的影响。结果表明,可以通过氩气压力来控制铝纳米粉的颗粒形状,大小和分布。高压氩气中制得的铝纳米颗粒具有较好的球形颗粒形状。同时,随着氩气压力的升高,铝纳米粉体的数均直径明显增加。较高压力的氩气可以明显拓宽铝纳米颗粒尺寸分布的范围。

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