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Efficient Detection of Edible Oils Adulterated with Used Frying Oils through PE-film-based FTIR Spectroscopy Combined with DA and PLS

机译:通过基于PE膜的FTIR光谱结合DA和PLS高效检测用过的煎炸油掺入的食用油

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摘要

Edible oil adulteration has been a considerable problem worldwide, and rapid detection methods should be established. In this study, a validation method for edible oil adulterated with used frying oil (UFO) was introduced through Fourier transform infrared (FTIR) spectroscopy. The spectral region of 6000-400 cm~(-1) was determined through FTIR by using a disposable polyethylene film, and absorption profiles at 1550-650 cm~(-1) region could be used for detection analysis. A qualitative analysis model was established through discriminant analysis, and edible oil adulteration with more than 1 % content of UFO could be qualitatively analyzed. A quantitative analysis model was also created through partial least squares regression. When the actual value was more than 1.5%, the predicted and actual values showed good linear correlation. FTIR coupled with chemometric analysis is a useful tool to detect edible oil adulteration.
机译:食用油掺假已成为世界范围内的一个严重问题,应建立快速检测方法。在这项研究中,通过傅里叶变换红外(FTIR)光谱法介绍了一种将用过的煎炸油(UFO)掺入食用油的验证方法。使用一次性聚乙烯薄膜通过傅立叶变换红外光谱(FTIR)确定了6000-400 cm〜(-1)的光谱范围,吸收光谱在1550-650 cm〜(-1)范围内可用于检测分析。通过判别分析建立了定性分析模型,可以对UFO含量在1%以上的食用油掺假进行定性分析。还通过偏最小二乘回归创建了定量分析模型。当实际值大于1.5%时,预测值和实际值显示出良好的线性相关性。 FTIR结合化学计量分析是检测食用油掺假的有用工具。

著录项

  • 来源
    《Journal of Oleo Science》 |2018年第9期|1083-1089|共7页
  • 作者单位

    College of Food Science and Engineering, Northwest A&F University, 22 Xinong Road Yangling, 712100 Shaanxi, P Ft CHINA;

    College of Food Science and Engineering, Northwest A&F University, 22 Xinong Road Yangling, 712100 Shaanxi, P Ft CHINA;

    College of Food Science and Engineering, Northwest A&F University, 22 Xinong Road Yangling, 712100 Shaanxi, P Ft CHINA;

    College of Food Science and Engineering, Northwest A&F University, 22 Xinong Road Yangling, 712100 Shaanxi, P Ft CHINA;

    College of Food Science and Engineering, Northwest A&F University, 22 Xinong Road Yangling, 712100 Shaanxi, P Ft CHINA;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    edible oils; FTIR; used frying oil; adulteration;

    机译:食用油;FTIR;用过的炸油;掺假;

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