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VALIDATION OF A HIGH PERFORMANCE LIQUID CHROMATOGRAPHY METHOD FOR CARBENDAZIM RESIDUES QUANTIFICATION IN TOMATOES

机译:高效液相色谱法在番茄中多菌灵残留量定量中的应用

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A high performance liquid chromatography method for carbendazim residues determination was adapted to the condition of our laboratory and validated for tomatoes samples. Carbendazim eluted at 3.13 minutes. The signal was linear over the concentration range 1 to 15 μg/ml with correlation coefficient 0.999092. The detection limit and the quantitation limit values were 0.002 mg/kg and 0.02 mg/kg respectively. Relative standard deviation of repeatability was 3.47% and 4.78% and recovery was 99.67% and 113,11% for two levels of concentration. The adapted method allowed a simple and rapid separation and quantification of carbendazim in tomatoes by high performance liquid chromatography.
机译:高效液相色谱法测定多菌灵残留量的方法适合于我们实验室的条件,并已针对番茄样品进行了验证。多菌灵在3.13分钟时洗脱。信号在1至15μg/ ml的浓度范围内呈线性,相关系数为0.999092。检出限为0.002 mg / kg,定量限为0.02 mg / kg。在两个浓度水平下,相对重复性的相对标准偏差分别为3.47%和4.78%,回收率分别为99.67%和113,11%。改进的方法可以通过高效液相色谱法简单,快速地分离和定量分析番茄中的多菌灵。

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