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Arsoma of Sparkling Wines by Headspace/Solid Phase Microextraction and Gas Chromatography/Mass Spectrometry

机译:顶空/固相微萃取和气相色谱/质谱法测定气泡酒的香气

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摘要

Aroma compounds of sparkling wines Cava (Certified Brand of Origin of Spain) were determined by Head- Space Solid Phase Microextraction (HS-SPME) using a 10-mm fiber coated with a 100-μm layer of polydimethylsiloxane. A rapid, easy, economic, and selective (without acid or alcohol interference) method was developed to analyze 17 flavor compounds of Cava. Five ethyl esters and two isoamyl esters, vitispirane and 2-dihydro-1,1,6-trimethyl-naphthalene (TDN), were quantified by the addition of an internal standard. These flavor components could be used to characterize sparkling wines with different periods of aging with yeast. Thus, aroma analysis by HS-SPME could be used to identify wines with the required nine-month aging (minimum legal aging for Cava sparkling wine) and to determine the approximate age of sparkling wines.
机译:使用顶空固相微萃取(HS-SPME),使用10毫米纤维涂有100微米的聚二甲基硅氧烷层,测定起泡酒Cava(西班牙原产地认证品牌)的香气成分。开发了一种快速,简便,经济和选择性(无酸或酒精干扰)的方法来分析卡瓦酒中的17种风味化合物。通过添加内标对5种乙基酯和2种异戊基酯(维斯匹灵和2-二氢-1,1,6-三甲基萘(TDN))进行定量。这些风味成分可用于表征具有不同陈酿期的起泡酒。因此,通过HS-SPME进行的香气分析可用于识别具有九个月陈年期(卡瓦起泡酒的最低法定陈年)的葡萄酒,并确定起泡酒的近似年龄。

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