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Removal of warmed-over flavor using absorbent and pattern recognition analysis of overall flavors by SPME-GC/MS-MVA.

机译:使用吸收剂去除变温的香料,并通过SPME-GC / MS-MVA对整体香料进行模式识别分析。

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摘要

The development of warmed-over flavor (WOF) was initially observed about 40 years ago, and it is now accepted to be the result of lipid oxidation, specifically oxidation of phospholipids in precooked meat during refrigerated storage. Because WOF continues to be one of the major quality concerns of pre-cooked meat products, studies of removing WOF from cooked meat still continue.; Our research was aimed at using an absorbent to remove WOF from cooked ground beef and to determine the resulting change in flavor profile by using Gas chromatography/mass spectrometry (GC/MS) as an e-nose (MS-only) as well as a traditional GC-MS.; A Carboxen/Polydimethylsiloxane (CAR/PDMS) SPME fiber was found to be the more appropriate fiber to extract beef flavors as compared to a Divinylbenzene/Carboxen/Polydimethylsiloxane (DVB/CAR/PDMS) fiber. Using the absorbent significantly reduced markers of WOF, such as pentanal, hexanal, heptanal and 2,3-octanedione. Changes in flavor profile pattern could be followed by traditional and e-nose GC-MS-MVA. Beef flavor volatiles, other than WOF compounds, changed to a lesser extent than oxidation products.; The results suggested that absorbent could have potential use in food packaging materials to absorb warmed-over flavor components. (Abstract shortened by UMI.)
机译:最初在40年前就观察到了变温香料(WOF)的发展,现在人们公认它是脂质氧化的结果,特别是冷藏存储过程中预煮肉中磷脂的氧化。因为WOF仍然是预煮肉制品的主要质量问题之一,所以从煮熟的肉中去除WOF的研究仍在继续。我们的研究旨在使用吸收剂从煮熟的绞碎的牛肉中去除WOF,并通过使用气相色谱/质谱(GC / MS)作为电子鼻(仅MS)以及通过使用气相色谱/质谱法确定风味变化的结果。传统的GC-MS。与二乙烯基苯/羧甲基/聚二甲基硅氧烷(DVB / CAR / PDMS)纤维相比,发现羧甲基/聚二甲基硅氧烷(CAR / PDMS)SPME纤维是更适合提取牛肉风味的纤维。使用吸收剂可显着降低WOF的标记物,例如戊醛,己醛,庚醛和2,3-辛二酮。传统和电子鼻GC-MS-MVA可以跟随风味特征模式的变化。除WOF化合物外,牛肉风味挥发物的变化程度小于氧化产物。结果表明,吸收剂在食品包装材料中具有潜在的用途,可以吸收变暖的风味成分。 (摘要由UMI缩短。)

著录项

  • 作者

    Li, Xifeng.;

  • 作者单位

    University of Missouri - Columbia.;

  • 授予单位 University of Missouri - Columbia.;
  • 学科 Chemistry Agricultural.; Agriculture Food Science and Technology.
  • 学位 M.S.
  • 年度 2004
  • 页码 86 p.
  • 总页数 86
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 农业化学;农产品收获、加工及贮藏;
  • 关键词

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