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Synthesis, Analysis, Transport and Field emission Measurements of Compound B-C-N Nanotubes

机译:化合物B-C-N纳米管的合成,分析,运输和场发射测量

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Multiwalled B-C-N nanotubes of various morphologies and chemical compositions were synthesized by reacting C-based nanotube templates with boron oxide and nitrogen at 1573 K-2173 K. The nanotubes were thoroughly analysed using a high-resolution field-emission 300 kV transmission electron microscope (TEM), an energy-filtered field-emission 300 kV electron microscope (Omega filter), an electron energy loss spectrometer and an energy dispersion X-ray detector. Transport and field emission properties of the nanotubes were studied using a low energy electron point source microscope and via in-situ measurements in TEM equipped with a scanning tunnelling microscope (STM) unit.
机译:通过在1573k-2173k中与氧化硼和氮使C基纳米管模板反应,合成各种形貌和化学组合物的多壁BCN纳米管。使用高分辨率场发射300kV透射电子显微镜(TEM)进行纳米管彻底分析纳米管),能量过滤场发射300kV电子显微镜(Omega滤波器),电子能损失光谱仪和能量分散X射线检测器。使用低能量电子点源显微镜和通过配备有扫描隧道显微镜(STM)单元的TEM的原位测量来研究纳米管的输送和场排放性能。

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