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Investigations on hydroxyapatite powder obtained by wet precipitation

机译:湿法沉淀法制备羟磷灰石粉的研究

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It is well-known that hydroxyapatite have multiple applications in tissue engineering due to compositional similarities with bone tissue. In this work, hydroxyapatite powders obtained by modified chemical precipitation route, has been investigated by AMF and SEM analysis grain size, X-ray diffraction and infra-red spectroscopy. The particle size of hydroxyapatite was observed to be very fine, uniform, around 50 -60 nm.rnSEM observation of the HA coatings showed the presence of nano-sized needles, with a significant level of agglomeration. The infrared analysis show the characteristic peaks of absorbed water, hydroxyl, phosphate and carbonate species. The XRD pattern clearly indicated the crystallites responsible for the Bragg reflection of the (002) and (003) planes are useful for size determination by Sherrer relationship (around 68 nm).
机译:众所周知,由于与骨组织的组成相似性,羟基磷灰石在组织工程中具有多种应用。在这项工作中,已经通过AMF和SEM分析晶粒度,X射线衍射和红外光谱研究了通过改进的化学沉淀途径获得的羟基磷灰石粉末。观察到羟基磷灰石的粒度非常细,均匀,大约在50 -60 nm处。rnSEM对HA涂层的观察表明存在纳米级针状物,并且具有显着的团聚水平。红外分析显示了吸收的水,羟基,磷酸盐和碳酸盐种类的特征峰。 XRD图清楚地表明,负责(002)和(003)平面布拉格反射的微晶对于通过Sherrer关系(约68 nm)确定尺寸非常有用。

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