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Synthesis and Characterization of Hydroxyapatite Powder by Wet Precipitation Method

机译:湿沉淀法合成与表征羟基磷灰石粉末

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Hydroxyapatite is main inorganic component of the bone with formula Ca_(10)(PO4)6(OH)2. Hydroxyapatite can be used as substituted bone biomaterial because biocompatible, non toxic, and osteoconductive. In this study, hydroxyapatite is synthesized using wet precipitation method from egg shell. The product was sintered at different temperatures of 800°C to 1000°C to improve its crystallinity. The hydroxyapatite was characterized by X-ray analysis, Scanning Electron Microscopy (SEM) and Fourier Transform Infrared Spectroscopy (FTIR) to reveal its phase content, morphology and types of bond present within it. The analytical results showed hydroxyapatite had range in crystallinity from 85.527 to 98.753%. The analytical functional groups showed that presence of functional groups such as OH, (PO4)_3~(2-) and CO_3~(2-) that indicated as hydroxyapatite. The result of characterization SEM indicated that hydroxyapatite without sintering and HAp sintering at 800 °C were irregular shape without pore. The best hydroxyapatite with temperature sintering at 900 °C showed oval shaped with pores without agglomerated.
机译:羟基磷灰石是骨的主要无机成分,配式Ca_(10)(PO4)6(OH)2。羟基磷灰石可用作取代的骨质材料,因为生物相容性,无毒和骨变性。在该研究中,使用来自蛋壳的湿沉淀法合成羟基磷灰石。将产物在800℃至1000℃的不同温度下烧结以改善其结晶度。羟基磷灰石的特征在于X射线分析,扫描电子显微镜(SEM)和傅里叶变换红外光谱(FTIR),以揭示其内部存在的相含量,形态和粘合类型。分析结果显示羟基磷灰石的结晶度范围从85.527〜98.753%。分析官能团表明,存在作为羟基磷灰石的官能团的存在,例如OH,(PO 4)_3〜(2-)和CO_3〜(2-)。表征SEM的结果表明,没有烧结的羟基磷灰石和800℃的HAP烧结是不规则的,没有孔隙。具有温度烧结的最佳羟基磷灰石在900℃下显示出椭圆形,孔隙无凝聚。

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