首页> 外国专利> METHOD OF PRODUCING POLYIMIDE RESIN METHOD OF PRODUCING POLYIMIDE COATING METHOD OF PRODUCING POLYAMIC ACID SOLUTION POLYIMIDE COATING AND POLYAMIC ACID SOLUTION

METHOD OF PRODUCING POLYIMIDE RESIN METHOD OF PRODUCING POLYIMIDE COATING METHOD OF PRODUCING POLYAMIC ACID SOLUTION POLYIMIDE COATING AND POLYAMIC ACID SOLUTION

机译:生产聚酰胺酸溶液聚酰亚胺涂层和聚酰胺酸溶液的聚酰亚胺涂布法生产聚酰亚胺树脂制备方法

摘要

[assignment] A method for producing a polyimide resin that provides a polyimide resin having excellent heat resistance and mechanical properties and a low dielectric constant even after heat treatment at a low temperature; a polyimide film manufacturing method that provides a polyimide film having excellent heat resistance and mechanical properties and a low dielectric constant even with heat treatment at a low temperature; a method for preparing a polyamic acid solution providing the polyimide resin; a polyimide film obtained by the method for producing a polyimide resin; And it provides a polyamic acid solution obtained by the method for preparing the polyamic acid solution. [Solution] In the method for producing a polyimide resin according to the present invention, a polyamic acid obtained by reacting a tetracarboxylic dianhydride component and a diamine component in a solvent containing at least the compound (A) represented by the following general formula (1) is heated at 120 to 350 ° C. including the process of In the formula, R 1 represents a hydrogen atom or a hydroxyl group, R 2 and R 3 independently represent a hydrogen atom or a C 1 toC 3 alkyl group, and R 4 and R 5 are independently C 1to C 3 represents an alkyl group.
机译:[任务]一种制备聚酰亚胺树脂的方法,其提供具有优异的耐热性和机械性能的聚酰亚胺树脂,即使在低温下热处理后也是低介电常数;一种聚酰亚胺膜制造方法,其提供具有优异的耐热性和机械性能的聚酰亚胺膜,即使在低温下的热处理也是如此的低介电常数;一种制备提供聚酰亚胺树脂的聚酰胺酸溶液的方法;通过制造聚酰亚胺树脂的方法获得的聚酰亚胺膜;它提供了通过制备聚酰胺酸溶液的方法获得的聚酰胺酸溶液。 [溶液]在根据本发明的制备聚酰亚胺树脂的制造方法中,通过将四羧酸二酐组分和二胺组分在含有下列通式所示的化合物(a)中的溶剂中反应而获得的聚酰胺酸(1 )在120至350℃下加热。包括在式中的方法,R 1表示氢原子或羟基,R 2和R 3独立地表示氢原子或C 1 TOC 3烷基,以及R图4和R 5独立地为C 1 C 3表示烷基。

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