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Improvements in or relating to the production of carbonaceous materials

机译:改进含碳材料的生产或与之相关的改进

摘要

A carbonaceous material is produced by forming a mixture of less than 5% by weight of cellulosic or hemicellulosic material and more then 95% of an aqueous liquid, e.g. pure water or water and a dispersing agent (zinc chloride), dispersing the material in the liquid by subjecting the mixture to mechanical beating for 30 minutes to 160 hours, regenerating the cellulosic or hemicellulosic material by removing free water from the dispersion, drying the regenerated material at a temperature below the boiling point of water at the pressure at which drying is effected and subjecting the dried material to a decomposition heat treatment, preferably at least partly under superatmospheric pressure, up to a final temperature of 400-2000 DEG C. in an inert atmosphere, e.g. nitrogen. The selections of starting material, heating time and heat treatment are such as to give a product with a bulk density of 0.2-1.6 grams per c.c. and a carbon content of 75-100% by weight. The starting material may be a -cellulose or a mixture of a -cellulose and hemicellulose containing at least 20% by weight hemicellulose, and drying may be at a temperature of at least 40 DEG and below 100 DEG C. under atmospheric pressure. The carbonaceous material may be shaped at the regeneration stage and machined after drying or at the completion of the heat treatment. The shaped bodies may be finally heated at a temperature from 2000-3000 DEG C.
机译:碳质材料是通过形成一种混合物来制成的,该混合物的重量百分比小于5%(纤维素或半纤维素材料),然后是95%以上的水性液体,例如纯水或水和分散剂(氯化锌),通过机械搅拌混合物30分钟至160小时将物料分散在液体中,通过从分散液中除去游离水再生纤维素或半纤维素物料,干燥再生的物料在低于进行干燥的压力下水的沸点的温度下对材料进行加热并使干燥的材料进行分解热处理,优选至少部分在超大气压下进行,直至最终温度为400-2000℃。惰性气氛,例如氮。起始原料,加热时间和热处理的选择使得得到的产品的堆积密度为每立方厘米0.2-1.6克。碳含量为75-100重量%。起始原料可以是含有至少20重量%半纤维素的α-纤维素或α-纤维素和半纤维素的混合物,并且在大气压下可以在至少40℃且低于100℃的温度下干燥。含碳材料可以在再生阶段成形,并在干燥后或在热处理完成后进行机加工。最终可以将成型体在2000-3000℃的温度下加热。

著录项

  • 公开/公告号GB1118626A

    专利类型

  • 公开/公告日1968-07-03

    原文格式PDF

  • 申请/专利权人 THE GENERAL ELECTRIC COMPANY LIMITED;

    申请/专利号GB19640043124

  • 发明设计人 LOSTY HOWARD HAROLD WALTER;

    申请日1964-10-22

  • 分类号C01B31/00;C04B35/524;

  • 国家 GB

  • 入库时间 2022-08-23 13:01:16

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