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Automatic analytical electron microscopy and analysis evaluation method

机译:自动分析电子显微镜及分析评价方法

摘要

PURPOSE: To automate measurement completely so as to facilitate analyzing operation by automatically recognizing the species, position and direction of the object to be analyzed and evaluated, and automatically adjusting an electron microscope. ;CONSTITUTION: When a specimen to be measured is mounted on a specimen holder 3 and inserted, an analyzing electron microscope is automatically set in an object recognizing operation by the control of a CPU 14. First, in searches the hole in the central part of the specimen, where transmission of an electron beam becomes the maximum, and begins observation from the vicinity of the hole. Next, it automatically increases its magnification in succession, and measures the intensity distribution of the transmitted electron beam. When variation in the intensity does not exceed a predetermined value, it is regarded as the same grain boundary, and the film thickness is automatically measured by means of an energy loss spectrometer 5 so as to judge the grain boundary. Finally, elementary analysis is carried out using an energy dispersion type X-ray analyzer 4, and adjustment is performed according to the distribution state of the intensity based on the element concentration. Consequently, a highly precise analysis can be easily carried out and analyzing time can be shortened.;COPYRIGHT: (C)1994,JPO&Japio
机译:目的:完全自动进行测量,以便通过自动识别要分析和评估的对象的种类,位置和方向,并自动调整电子显微镜来促进分析操作。 ;构成:将要测量的样本安装在样本支架3上并插入时,通过CPU 14的控制,自动将分析电子显微镜设置在物体识别操作中。首先,在电子显微镜的中央部分寻找孔电子束的透射达到最大的样品,从孔附近开始观察。接下来,它会自动连续放大倍率,并测量透射电子束的强度分布。当强度的变化不超过预定值时,将其视为相同的晶界,并且通过能量损失光谱仪5自动测量膜厚度以判断晶界。最后,使用能量分散型X射线分析仪4进行元素分析,并根据基于元素浓度的强度的分布状态进行调整。因此,可以很容易地进行高精度分析,并且可以缩短分析时间。;版权所有:(C)1994,日本特许厅&日本apio

著录项

  • 公开/公告号JP2777505B2

    专利类型

  • 公开/公告日1998-07-16

    原文格式PDF

  • 申请/专利权人 HITACHI SEISAKUSHO KK;

    申请/专利号JP19920202314

  • 发明设计人 AOYAMA TAKASHI;MISAWA YUTAKA;

    申请日1992-07-29

  • 分类号H01J37/26;H01J37/295;

  • 国家 JP

  • 入库时间 2022-08-22 03:01:41

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