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REACTOR AND SYSTEM FOR FABRICATION OF FREE-STANDING TWO-DIMENSIONAL NANOSTRUCTURES USING PLASMA TECHNOLOGY

机译:利用等离子体技术制造自由二维纳米结构的反应器和系统

摘要

The present invention relates to a process, reactor and system to produce self-standing two-dimensional nanostructures, using a microwave-excited plasma environment. The process is based on injecting, into a reactor, a mixture (9) of gases and precursors in stream regime. The stream is subjected to a surface wave (5) electric field, excited by the use of microwave power (7) which is introduced into a field applicator (6), generating high energy density plasmas (2,3,4), that break the precursors into its atomic and/or molecular constituents. The system comprises a plasma reactor with a surface wave launching zone, a transient zone with a progressively increasing cross-sectional area, and a nucleation zone. The plasma reactor together with an infrared radiation source (11) provides a controlled adjustment of the spatial gradients, of the temperature and the gas stream velocity. The majority of the obtained two-dimensional nanostructures samples have a thickness of a single atomic layer, in addition the process and system allow to obtain graphene production rates of the order of one gram per hour and higher.
机译:本发明涉及利用微波激发等离子体环境产生自立二维纳米结构的方法,反应器和系统。该方法基于以流态将气体和前体的混合物(9)注入到反应器中。气流受到表面波(5)电场的作用,该电场通过使用微波功率(7)激发而被引入场施加器(6)中,从而产生高能密度等离子体(2,3,4),该等离子体破裂将前体转变成其原子和/或分子成分。该系统包括具有表面波发射区,具有逐渐增大的横截面积的瞬态区和成核区的等离子体反应器。等离子体反应器与红外辐射源(11)一起提供了空间梯度,温度和气流速度的受控调节。获得的大多数二维纳米结构样品具有单原子层的厚度,此外,该方法和系统允许获得每小时1克左右或更高的石墨烯生产率。

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