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The method for preparation of polyvinylidene fluoride nanoparticle using polyethylene glycols and the polyvinylidene fluoride nanoparticle thereby

机译:使用聚乙二醇制备聚偏氟乙烯纳米颗粒的方法和由此得到的聚偏氟乙烯纳米颗粒

摘要

Preparing a mixed solution by mixing a radical initiator, distilled water, and a compound represented by the following Chemical Formula 1 in one aspect of the present invention (step 1); And adding vinylidene fluoride (VDF) to the mixed solution prepared in step 1 (step 2); providing a method of manufacturing polyvinylidene fluoride (PVDF) nanoparticles do. The method for producing polyvinylidene fluoride nanoparticles according to the present invention is a process using an existing ammonium-based surfactant (ammonium perfluorinated octanoate, APFO) having 8 carbon fluoride by using a polyethylene glycol-based compound for emulsion polymerization. Not only can it be used in a much smaller amount, the compound used in the present invention has an effect that can reduce the manufacturing cost of polyvinylidene fluoride as well as APFO replacement because there is little human accumulation and toxicity.
机译:在本发明的一个方面中,通过混合自由基引发剂,蒸馏水和以下化学式1表示的化合物来制备混合溶液(步骤1);然后将偏二氟乙烯(VDF)加入步骤1中制备的混合溶液中(步骤2);提供一种制造聚偏氟乙烯(PVDF)纳米颗粒的方法。根据本发明的制备聚偏二氟乙烯纳米颗粒的方法是使用现有的具有8个氟化碳的铵基表面活性剂(全氟化辛酸铵,APFO)通过将聚乙二醇基化合物用于乳液聚合的方法。本发明所使用的化合物不仅可以以更少的量使用,而且由于几乎没有人的积累和毒性,因此具有可以降低聚偏二氟乙烯的制造成本以及代替APFO的效果。

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