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New Application of Bromotrimethylsilane: Elaboration of Aldehydes/ Ketones into Homologous Alpha-Beta-Unsaturated Esters via Beta-Hydroxy Esters

机译：Bromotrimethylsilane的新应用：通过β-羟基酯将醛/酮配制成同系的α-β-不饱和酯

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摘要

Alpha,beta-unsaturated ester is formed when beta-hydroxy-ester is reacted with bromotrimethylsilane generated from chlorotrimethylsilane-lithium bromide in acetonitrile.

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作者
Suri, S. C. ; Marcischak, J. C.;
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年度 2003
页码 1-7
总页数 7
原文格式 PDF
正文语种 eng
中图分类工业技术;
关键词
Aldehydes; Ketones; Acetonitrile; Synthesis(Chemistry); Silanes; Esters;

机译：醛;酮;乙腈;合成（化学），硅烷，酯;

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1. New Application of Bromotrimethylsilane:Elaboration of Aldehydes/Ketones into Homologous alpha,beta-Unsaturated Esters via beta-Hydroxy Esters [J] . Suresh C.Suri, Jacob C.Marcischak Synthetic Communications . 2005,第3期

机译：溴三甲基硅烷的新应用：通过β-羟基酯将醛/酮加工成同源的α，β-不饱和酯
2. Mild and direct conversion of esters to morpholine amides using diisobutyl(morpholino)aluminum: application to efficient one-pot synthesis of ketones and aldehydes from esters [J] . Ah Ram Jeon, Min Eai Kim, Jae Kyo Park, Tetrahedron . 2014,第29期

机译：使用二异丁基（吗啉代）铝将酯轻度和直接转化为吗啉酰胺：应用于从酯高效一锅合成酮和醛
3. Dynamic headspace analysis of the light-induced controlled release of perfumery aldehydes and ketones from #alpha#-keto esters in bodycare and household applications [J] . Andreas Herrmann, Christian Debonneville, Valerie Laubscher, Flavour and Fragrance Journal . 2000,第6期

机译：在个人护理和家用应用中，光诱导的＃alpha＃-酮酸酯中香料醛和酮的受控释放的动态顶空分析
4. Efficient Synthesis of α,β-Unsaturated Esters from Aldehydes and Ketones with α,α-Bis(dimethylsilyl)esters [C] . Katsukiyo Miura, Masaru Ebine, Junji Ichikawa Symposium on Organometallic Chemistry . 2008

机译：用α，α-BIS（二甲基甲硅烷基）酯的醛和酮的α，β-不饱和酯的高效合成
5. The epoxidation of dienes, alpha,beta-unsaturated ketones, alpha,beta-unsaturated esters and vinyl esters by dimethyldioxirane. [D] . Chen, Hsinhung. 2001

机译：二烯，α，β-不饱和酮，α，β-不饱和酯和乙烯基酯被二甲基二环氧乙烷环氧化。
6. Scientific Opinion on Flavouring Group Evaluation 63 Revision 3 (FGE.63Rev3): aliphatic secondary alcohols ketones and related esters evaluated by JECFA (59th and 69th meetings) structurally related to saturated and unsaturated aliphatic secondary alcohols ketones and esters of secondary alcohols and saturated linear or branched‐chain carboxylic acids evaluated by EFSA in FGE.07Rev4 [O] . EFSA Panel on Food Contact Materials, Enzymes, Flavourings and Processing Aids (CEF), 2017

机译：关于调味组评估63的科学意见修订版3（FGE.63Rev3）：JECFA（第五十九次和第六十九次会议）评估的脂肪族仲醇酮和相关酯的结构与饱和和不饱和脂肪族仲醇酮和仲醇的酯有关由EFSA在FGE.07Rev4中评估的饱和直链或支链羧酸
7. Studies in Alcoholysis IV. The Alcoholysisof Esters of alpha-beta-unsaturated acids and of the corresponding saturated esters [O] . Dasannacharya B, Sudborough JJ 1921

机译：醇解研究IV。 α-β-不饱和酸和相应饱和酯的酯的醇解

New Application of Bromotrimethylsilane: Elaboration of Aldehydes/ Ketones into Homologous Alpha-Beta-Unsaturated Esters via Beta-Hydroxy Esters

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