Analyses of Explosives. Physical-Chemical Data, Chromatograms, Mass-, IR- and NMR-Spectra. Colour Reactions and Thin Layer Chromatography

摘要

Literature searches on identification and analyses of explosives have shown that there is no comprehensive report on analytical methods for this group of substances. (A recently published review is Yinon, J: Analysis of explosives. CRC Crit Rev Anal Chem 7 (1977) 1-35.) Due to this fact the present work was carried out. The report comprises spectra and chromatograms of 25 substances of which eleven are frequently used explosives and the remaining fourteen are nitrotoluene isomers. Instrumental methods have been applied. The spectral analyses include mass spectrometry (electron impact, chemical ionization), infrared spectrometry and nuclear magnetic resonance. The chromatographic analyses include gas chromatography and high pressure liquid chromatography. Data on instrumentation and experimental conditions are given in each chapter. (Author)