Synthesis of 1-(2,6-dimethylphenyl)-N-hydroxy-4,4-dialkyl-2,5-dioxo-N-aryl-3-pyrrolid ine-carboxamides from reaction of 2,6-dimethylphenyl isocyanide, alkylidene Meldrum's acids, and arylhydroxylamines

Habibi A; Mousavifar L; Yazdanbakhsh MR; Yavari I

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Synthesis of 1-(2,6-dimethylphenyl)-N-hydroxy-4,4-dialkyl-2,5-dioxo-N-aryl-3-pyrrolid ine-carboxamides from reaction of 2,6-dimethylphenyl isocyanide, alkylidene Meldrum's acids, and arylhydroxylamines

机译：由2,6-二甲基苯基异氰化物与亚烷基Meldrum's反应合成1-（2,6-二甲基苯基）-N-羟基-4,4-二烷基-2,5-二氧代-N-芳基-3-吡咯烷-氨基酰胺酸和芳基羟胺

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摘要

Alkylidene Meldrum's acids and 2,6-dimethylphenyl isocyanide react smoothly in the presence of arylhydroxylamines at room temperature to produce 2,5-dioxo-pyrrolidines in fairly high yield.

机译：在室温下，在芳基羟胺的存在下，亚炔基Meldrum的酸与2,6-二甲基苯基异氰化物能平稳反应，从而以相当高的收率生产2,5-二氧-吡咯烷。

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《Synthetic Communications》 |2008年第6期|共8页
作者
Habibi A; Mousavifar L; Yazdanbakhsh MR; Yavari I;
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正文语种 eng
中图分类有机化学;
关键词
alkylidene Meldrum's acid; 2; 5-dioxopyrrolidine; heterocyclic synthesis; isocyanide; three-component reaction;

机译：亚烷基Meldrum's acid;2;5-二氧杂吡咯烷;杂环合成;异氰化物;三组分反应;

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1. Synthesis of 1-(2,6-dimethylphenyl)-N-hydroxy-4,4-dialkyl-2,5-dioxo-N-aryl-3-pyrrolid ine-carboxamides from reaction of 2,6-dimethylphenyl isocyanide, alkylidene Meldrum's acids, and arylhydroxylamines [J] . Habibi A, Mousavifar L, Yazdanbakhsh MR, Synthetic Communications . 2008,第4a6期

机译：由2,6-二甲基苯基异氰化物与亚烷基Meldrum's反应合成1-（2,6-二甲基苯基）-N-羟基-4,4-二烷基-2,5-二氧代-N-芳基-3-吡咯烷-氨基酰胺酸和芳基羟胺
2. Synthesis of 1-(2,6-Dimethylphenyl)-N-hydroxy-4,4-dialkyl-2,5-dioxo-N-aryl-3-pyrrolidine-carboxamides from Reaction of 2,6-Dimethylphenyl Isocyanide, Alkylidene Meldrum's Acids, and Arylhydroxylamines [J] . Synthetic Communications . 2008,第6期

机译：由2,6-二甲基苯基异氰酸酯与亚烷基Mel的酸反应合成1-（2,6-二甲基苯基）-N-羟基-4,4-二烷基-2,5-二氧代-N-芳基-3-吡咯烷-甲酰胺和芳基羟胺
3. Synthesis of 1-(2,6-dimethylphenyl)-N-hydroxy-4,4-dialkyl-2,5-dioxo-N-aryl-3-pyrrolidine-carboxamides from reaction of 2,6-dimethylphenyl isocyanide, alkylidene Meldrum's acids, and arylhydroxylamines [J] . Habibi A, Mousavifar L, Yazdanbakhsh MR, Synthetic Communications . 2008,第6期

机译：由2,6-二甲基苯基异氰化物与亚烷基Meldrum's酸反应合成1-（2,6-二甲基苯基）-N-羟基-4,4-二烷基-2,5-二氧代-N-芳基-3-吡咯烷-羧酰胺和芳基羟胺
4. Synthesis, Structural, Spectroscopic, and Morphology of Metal-Organic Frameworks Based on La(III)and Ligand 2,6-Napthalenedicarboxylic acid(La-MOFs)for Hydrogen Production [C] . Ninda Hardina Batubara, Agustino Zulys Annual Basic Science International Conference . 2019

机译：基于La（III）和配体2,6-萘二甲酸（La-MOF）的金属 - 有机骨架的合成，结构，光谱和形态，用于氢气产生
5. A chemical-enzymatic method for the synthesis of sialylated oligosaccharides: Synthesis of cytidine monophosphate-sialic acid analogs for use in probing the donor specificity of alpha-2,3- and alpha-2,6-sialyltransferase. [D] . Chappell, Mark Donald. 1999

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6. Synthesis of a novel category of pseudo-peptides using an Ugi three-component reaction of levulinic acid as bifunctional substrate amines and amino acid-based isocyanides [O] . Maryam Khalesi, Azim Ziyaei Halimehjani, Jürgen Martens 2019

机译：使用乙酰丙酸的乌吉三组分反应作为双功能底物胺和氨基酸基异氰酸酯合成新型伪肽
7. Estrogenic action by tris(2,6-dimethylphenyl) phosphate, an impurity in resorcinol bisdi(2,6-dimethylphenyl) phosphate flame retardant formulations, impairs the development of female reproductive functions [O] . Kazuhiro Sano, Hidenori Matsukami, Go Suzuki, 2019

机译：Tris（2,6-二甲基苯基）磷酸酯的雌激素作用，间苯二酚双（2,6-二甲基苯基）磷酸酯的杂质阻燃配方，损害了雌性生殖功能的发展

Synthesis of 1-(2,6-dimethylphenyl)-N-hydroxy-4,4-dialkyl-2,5-dioxo-N-aryl-3-pyrrolid ine-carboxamides from reaction of 2,6-dimethylphenyl isocyanide, alkylidene Meldrum's acids, and arylhydroxylamines

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