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Optimization of process parameters to maximize hardness of metal/ceramic nanocomposites produced by high energy ball milling

机译:优化工艺参数以最大程度地提高高能球磨生产的金属/陶瓷纳米复合材料的硬度

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摘要

In our previous work [Abdellahi, J. Mater. Res. 28 (2013) 3270], a novel method was used to predict the hardness of Aluminum matrix nanocomposites synthesized by high energy ball milling. In the mentioned work, however, systems under study were very limited, the squared regression of training and testing sets was not significant and optimizing was not performed on the milling parameters so that we finally had not an optimal system with a maximum value of hardness. In this work, for the first time, all mentioned shortcomings were addressed and resolved and as a new work the process parameters, namely, amount of reinforcement, amount of process control agent, type of mill, type of vial, type of ball, vial spinning rate, ball to powder weight ratio, type of process control agent, type of atmosphere, milling time, sintering time, sintering temperature and compact pressure were optimized to maximize the hardness of metal/ceramic nanocomposites produced by high energy ball milling. To evaluate the efficiency of the proposed optimization, a system based on the optimized parameters was established (system 2) and the obtained results were compared with those in system that was established based on the parameters used by Akbarpour et al. (system 1). The results showed two things: first, the use of system 2 brings a maximum value of hardness for the produced nanocomposites and second, the optimized system is really consistent with what actually happens in practice.
机译:在我们以前的工作中[Abdellahi,J. Mater。 Res。 28(2013)3270],一种新方法被用来预测通过高能球磨合成的铝基纳米复合材料的硬度。但是,在上述工作中,所研究的系统非常有限,训练和测试集的平方回归并不显着,并且未对铣削参数进行优化,因此我们最终没有一个具有最大硬度值的最佳系统。在这项工作中,首次解决了所有提到的缺点并解决了这些问题,并且作为一项新工作,工艺参数,即补强量,过程控制剂的用量,研磨机的类型,小瓶的类型,球的类型,小瓶的类型优化了纺丝速度,球与粉末的重量比,工艺控制剂的类型,气氛的类型,研磨时间,烧结时间,烧结温度和压制压力,以使通过高能球磨生产的金属/陶瓷纳米复合材料的硬度最大化。为了评估所提出优化的效率,建立了基于优化参数的系统(系统2),并将获得的结果与基于Akbarpour等人使用的参数建立的系统中的结果进行了比较。 (系统1)。结果表明两件事:首先,系统2的使用为所生产的纳米复合材料带来了最大的硬度值,其次,优化后的系统与实践中的实际情况完全一致。

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