Convenient Method for Determination of Optical Purity of Chiral Alcohols and Amines

V.V.Nesterov; E.V.Grishkun; O.I.Kolodyazhnyi

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Convenient Method for Determination of Optical Purity of Chiral Alcohols and Amines

机译：测定手性醇和胺的光学纯度的简便方法

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Chemical transformation of chiral compounds serves as an important method of determination of their optical purity,and it has been widely explored over the past years [1-5].We found that di-( lR,2S,5R)-menthyl phosphoro-chloridite (I) is a convenient reagent for the determination of optical purity of chiral alcohols and amines by ~(31)P NMR spectroscopy.

机译：手性化合物的化学转化是测定其光学纯度的重要方法，并且在过去的几年中已被广泛研究[1-5]。我们发现二-（lR，2S，5R）-薄荷基次氯代亚氯酸盐（I）是通过〜（31）P NMR光谱测定手性醇和胺的光学纯度的便捷试剂。

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《Russian Journal of General Chemistry》 |2004年第12期|共2页
作者
V.V.Nesterov; E.V.Grishkun; O.I.Kolodyazhnyi;
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中图分类化学;
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1. Convenient Method for Determination of Optical Purity of Chiral Alcohols and Amines [J] . V.V.Nesterov, E.V.Grishkun, O.I.Kolodyazhnyi Russian Journal of General Chemistry . 2004,第12期

机译：测定手性醇和胺的光学纯度的简便方法
2. First principles design of derivatizing agent for direct determination of enantiomeric purity of chiral alcohols and amines by NMR spectroscopy [J] . Nikolay V. Orlov, Valentine P. Ananikov Chemical Communications . 2010,第18期

机译：NMR光谱法直接测定手性醇和胺的对映体纯度的衍生剂的第一原理设计
3. O-Methylatrolactic acid as a new reagent for determination of the enantiomeric purity and absolute configuration of chiral alcohols and amines [J] . Kowalczyk R, Skarzewski J Tetrahedron, Asymmetry: The International Journal for Repid Publication on all Aspects of Asymmetry in Orgainc, Inorganic, Organometallic, Physical and Bio-Organic Chemistry . 2006,第9期

机译：邻甲基正丙酸作为测定手性醇和胺的对映体纯度和绝对构型的新试剂
4. A NEW CHIRAL PHOSPHOROUS AGENT FOR THE DETERMINATION OF THE ENANTIOMERIC EXCESS OF CHIRAL ALCOHOLS,AMINES BY MEANS OF 31p NMR [C] . Li Kangying International symposium for Chinese organic chemists . 2000

机译：一种新的手性磷剂，用于测定对映体过量的手性醇，胺含31P NMR的胺
5. Determination of the Absolute Configuration of β-Chiral Primary Alcohols Using the Competing Enantioselective Conversion Method Heteroatom-directed Acylation of Secondary Alcohols to Assign Absolute Configuration Total Synthesis of Illisimonin a Osmate Es [D] . Burns, Alexander Sunshine. 2020

机译：使用竞争对映选择性转化法测定β-chiral初级醇的绝对构型次原子为仲醇的酰化酰化，分配绝对构型Illisimonin的总合成渗透
6. Determination of Optical Purity of Lactic Acid-Based Chiral Liquid Crystals and Corresponding Building Blocks by Chiral High-Performance Liquid Chromatography and Supercritical Fluid Chromatography [O] . Anna Poryvai, Terezia Vojtylová-Jurkovičová, Michal Šmahel, 2019

机译：手性高效液相色谱和超临界流体色谱法测定乳酸基手性液晶及其相应结构单元的光学纯度
7. APPLICATION OF OPTICALLY ACTIVE ORGANOSILANE TO THE DETERMINATION OF OPTICAL PURITIES OF AMINES, ALCOHOLS, AND CARBOXYLIC ACIDS [O] . Daiyo Terunuma, Masato Kato, Masanao Kamei, 1985

机译：光学活性有机硅烷在胺，醇和羧酸的光学纯度测定中的应用
8. Spectroscopic Method for the Determination of Optical Purities of Chiral, Chelating Diphosphines. [R] . Kyba, E. P., Rines, S. P. 1982

机译：光谱法测定手性螯合二膦的光学纯度。

Convenient Method for Determination of Optical Purity of Chiral Alcohols and Amines

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