Clay Supported Bis(trimethylsilyl) chromate: Oxidative Deprotection of Tetrahydropyranyl Ethers under Solvent-Free Conditions using Microwaves

Majid M. Heravi; Dariush Ajami

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Clay Supported Bis(trimethylsilyl) chromate: Oxidative Deprotection of Tetrahydropyranyl Ethers under Solvent-Free Conditions using Microwaves

机译：粘土支撑的双（三甲基甲硅烷基）铬酸盐：四氢吡喃基醚在无溶剂条件下的微波氧化脱保护

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摘要

Tetrahydropyranyl ethers are rapidly and selectively oxidized to the corresponding carbonyl compounds by montmorillonite K-10 supported bis(trimethylsilyl) chromate under solventfree conditions using microwaves.

机译：在无溶剂条件下，使用微波，由蒙脱石K-10负载的双（三甲基甲硅烷基）铬酸盐将四氢吡喃基醚快速选择性地氧化为相应的羰基化合物。

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《Monatshefte fur Chemie》 |1999年第5期|共4页
作者
Majid M. Heravi; Dariush Ajami;
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正文语种 eng
中图分类化学;
关键词
clay supported reagent; oxidation; deprotection; dehydropyranylation;

机译：粘土负载试剂;氧化;脱保护;脱氢吡喃基化;

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1. Clay Supported Bis(trimethylsilyl) chromate: Oxidative Deprotection of Tetrahydropyranyl Ethers under Solvent-Free Conditions using Microwaves [J] . Majid M. Heravi, Dariush Ajami Monatshefte fur Chemie . 1999,第5期

机译：粘土支撑的双（三甲基甲硅烷基）铬酸盐：四氢吡喃基醚在无溶剂条件下的微波氧化脱保护
2. An easy and fast method for oxidative deprotection of trimethylsilyl ethers,tetrahydropyranyl ethers,and ethylene acetals with KMnO_4 supported on alumina under solvent-free conditions [J] . A.R.Haijipour, S.E.Mallakpour, I.M.Baltork, Synthetic Communications . 2002,第5期

机译：在无溶剂条件下用氧化铝上负载的KMnO_4对三甲基甲硅烷基醚，四氢吡喃基醚和乙缩醛进行氧化脱保护的简便快捷方法
3. HNO3/Silica gel supported CAN; oxidative deprotection of benzylic tetrahydropyranyl ethers under solvent-free conditions using microwaves [J] . Heravi MM, Kazemian P, Oskooie HA, Journal of Chemical Research. Synopses . 2005,第2期

机译：HNO3 /硅胶支持的CAN;在无溶剂条件下使用微波对苄基四氢吡喃基醚进行氧化脱保护
4. Silica Supported Barium Chloride (SiO2-BaCl2): Efficient and Heterogeneous catalyst for the environmentally friendly preparation of N,N′-alkylidene bisamides under solvent-free condition [C] . 2nd International Conference on Chemical, Biological and Environmental Engineering . 2010

机译：二氧化硅负载的氯化钡（SiO 2 -BaCl 2 ）：高效，多相催化剂，可在无溶剂条件下环保地制备N，N'-亚烷基双酰胺
5. Tandem mass spectrometry: Gas-phase ion chemistry for the identification of fragmentation pathways of bis(trimethylsilyl) ethers and the determination of structural isomers of carcinogen-DNA adducts. [D] . Byun, Jaeman. 1996

机译：串联质谱：气相离子化学法，用于鉴定双（三甲基甲硅烷基）醚的裂解途径，并确定致癌物-DNA加合物的结构异构体。
6. Sulphated Zirconia as an Eco-Friendly Catalyst in Acylal Preparation under Solvent-Free Conditions Acylal Deprotection Assisted by Microwaves and the Synthesis of Anhydro-Dimers of o-Hydroxybenzaldehydes [O] . Laura Nadxieli Palacios-Grijalva, Deysi Y. Cruz-González, Leticia Lomas-Romero, 2009

机译：无溶剂条件下硫酸盐化氧化锆在制备酰基中的环保催化剂微波辅助的酰基脱保护和邻羟基苯甲醛脱水二聚体的合成
7. An Efficient Method for Selective Deprotection of Trimethylsilyl Ethers and Tetrahydropyranyl Ethers under Solvent-free Conditions [O] . 2005

机译：在无溶剂条件下选择性脱保护三甲基甲硅烷基醚和四氢吡喃基醚的有效方法

Clay Supported Bis(trimethylsilyl) chromate: Oxidative Deprotection of Tetrahydropyranyl Ethers under Solvent-Free Conditions using Microwaves

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