HNO3/Silica gel supported CAN; oxidative deprotection of benzylic tetrahydropyranyl ethers under solvent-free conditions using microwaves

Heravi MM; Kazemian P; Oskooie HA; Ghassemzadeh M

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HNO3/Silica gel supported CAN; oxidative deprotection of benzylic tetrahydropyranyl ethers under solvent-free conditions using microwaves

机译：HNO3 /硅胶支持的CAN;在无溶剂条件下使用微波对苄基四氢吡喃基醚进行氧化脱保护

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摘要

Benzylic tetrahydropyranyl ethers are rapidly and selectively oxidised to the corresponding carbonyl compounds by HNO3/silica gel supported cerium ammonium nitrate (CAN) under solvent free conditions using microwave.

机译：在无溶剂条件下，使用微波，通过HNO3 /硅胶负载的硝酸铈铵铵（CAN），将苄基四氢吡喃基醚快速选择性地氧化为相应的羰基化合物。

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《Journal of Chemical Research. Synopses》 |2005年第2期|共2页
作者
Heravi MM; Kazemian P; Oskooie HA; Ghassemzadeh M;
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正文语种 eng
中图分类化学;
关键词
CAN; oxidative deprotection; THP ethers; CERIUM(IV) AMMONIUM-NITRATE; ORGANIC-REACTIONS; REAGENTS;

机译：CAN;氧化脱保护;THP醚;硝酸铈铵;有机反应;试剂;

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1. HNO3/Silica gel supported CAN; oxidative deprotection of benzylic tetrahydropyranyl ethers under solvent-free conditions using microwaves [J] . Heravi MM, Kazemian P, Oskooie HA, Journal of Chemical Research. Synopses . 2005,第2期

机译：HNO3 /硅胶支持的CAN;在无溶剂条件下使用微波对苄基四氢吡喃基醚进行氧化脱保护
2. Direct oxidative deprotection of tetrahydropyranyl ethers using hexamethylenetetramine-bromine supported onto silica gel under microwave irradiation in solventless system [J] . Dehkordi MB, Heravi MM, Ziafati A, Phosphorus, Sulfur, and Silicon and the Related Elements . 2004,第8期

机译：无溶剂体系中微波辐射下载于硅胶上的六亚甲基四胺-溴对四氢吡喃基醚的直接氧化脱保护
3. An easy and fast method for oxidative deprotection of trimethylsilyl ethers,tetrahydropyranyl ethers,and ethylene acetals with KMnO_4 supported on alumina under solvent-free conditions [J] . A.R.Haijipour, S.E.Mallakpour, I.M.Baltork, Synthetic Communications . 2002,第5期

机译：在无溶剂条件下用氧化铝上负载的KMnO_4对三甲基甲硅烷基醚，四氢吡喃基醚和乙缩醛进行氧化脱保护的简便快捷方法
4. Silica gel-mediated hydrohalogenation of alkenes using hydrohalogenic acids under solvent-free conditions [C] . Kiyoshi Tanemura 日本化学会春季年会講演予稿集 . 2018

机译：在无溶剂条件下使用氢卤代酸硅胶介导的烯烃的含水氢化物
5. Microwave-enhanced Processing of Transition Metal oxides, Silicates, and Aluminosilicates and Their Catalytic Studies. [D] . Opembe, Naftali Nandera. 2012

机译：过渡金属氧化物，硅酸盐和铝硅酸盐的微波增强处理及其催化研究。
6. Sulphated Zirconia as an Eco-Friendly Catalyst in Acylal Preparation under Solvent-Free Conditions Acylal Deprotection Assisted by Microwaves and the Synthesis of Anhydro-Dimers of o-Hydroxybenzaldehydes [O] . Laura Nadxieli Palacios-Grijalva, Deysi Y. Cruz-González, Leticia Lomas-Romero, 2009

机译：无溶剂条件下硫酸盐化氧化锆在制备酰基中的环保催化剂微波辅助的酰基脱保护和邻羟基苯甲醛脱水二聚体的合成
7. An Efficient Method for Selective Deprotection of Trimethylsilyl Ethers and Tetrahydropyranyl Ethers under Solvent-free Conditions [O] . 2005

机译：在无溶剂条件下选择性脱保护三甲基甲硅烷基醚和四氢吡喃基醚的有效方法

HNO3/Silica gel supported CAN; oxidative deprotection of benzylic tetrahydropyranyl ethers under solvent-free conditions using microwaves

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