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Qualitative and quantitative determination of YiXinShu Tablet using ultra high performance liquid chromatography with Q Exactive hybrid quadrupole orbitrap high‐resolution accurate mass spectrometry

机译：用Q辐射杂交四轴绕高分辨率精确质谱法用超高效液相色谱法定性和定量测定益征液相色谱法

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Abstract > To clarify and quantify the chemical profile of YiXinShu Tablet rapidly, a feasible and accurate strategy was developed by applying ultra high performance liquid chromatography with Q Exactive hybrid quadrupole orbitrap high‐resolution accurate mass spectrometry. A total of 105 components were identified, including 25 phenanthraquinones, 11 lactones, 19 lignans, 24 acids, and 26 other compounds. Among them, 26 major compounds were unambiguously detected by comparing with reference standards. And 19 of these compounds in three batches of YiXinShu Tablet were selected for quantitative determination. ( Z )‐Ligustilide, salvianic acid A, salvianolic acid A, salvianolic acid B, and rosmarinic acid were abundant in these three batches with contents over 1?mg/g. The established analysis methods were examined to be accurate and feasible. The results show that the ultra high performance liquid chromatography with Q Exactive hybrid quadrupole orbitrap high‐resolution accurate mass spectrometry method has a powerful qualitative ability and promising quantitative application. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>摘要</ title> >迅速澄清和量化yixinshu平板电脑的化学特征，开发了一种可行和准确的策略通过将超高效液相色谱法与Q辐射活性杂交四孔玻璃高分辨率高分辨率施加高分辨率。鉴定了总共105个组分，包括25个菲醌，11个乳酰胺，19只木质藻，24酸和26种其他化合物。其中，通过与参考标准进行比较，可以明确地检测26种主要化合物。选择了三种易西岛片中的19种化合物，用于定量测定。（ Z </ i>）--ligustilide，Salvian acid A，Salvianolic acid A，Salvianolic acid B和rosmarinic在这三个批次中丰富，内容物超过1？Mg / g。预先检查建立的分析方法是准确和可行的。结果表明，具有Q辐射杂交四轴壁图高分辨率精确质谱法的超高效液相色谱具有强大的定性能力和有前途的定量应用。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35800/'>《Journal of separation science.》</a> <b style="margin: 0 2px;">|</b><span>2017年第22期</span><b style="margin: 0 2px;">|</b><span>共14页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sun Zhi&option=202" target="_blank" rel="nofollow">Sun Zhi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Zhuolun&option=202" target="_blank" rel="nofollow">Li Zhuolun;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zuo Lihua&option=202" target="_blank" rel="nofollow">Zuo Lihua;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Zhenhui&option=202" target="_blank" rel="nofollow">Wang Zhenhui;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhou Lin&option=202" target="_blank" rel="nofollow">Zhou Lin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shi Yingying&option=202" target="_blank" rel="nofollow">Shi Yingying;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kang Jian&option=202" target="_blank" rel="nofollow">Kang Jian;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhu Zhenfeng&option=202" target="_blank" rel="nofollow">Zhu Zhenfeng;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Xiaojian&option=202" target="_blank" rel="nofollow">Zhang Xiaojian;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of PharmacyThe First Affiliated Hospital of Zhengzhou UniversityZhengzhou P. R. China;</p> <p>Department of PharmacyThe First Affiliated Hospital of Zhengzhou UniversityZhengzhou P. R. China;</p> <p>Department of PharmacyThe First Affiliated Hospital of Zhengzhou UniversityZhengzhou P. R. China;</p> <p>College of MedicineHenan Polytechnic UniversityJiaozuo P. R. China;</p> <p>Department of PharmacyThe First Affiliated Hospital of Zhengzhou UniversityZhengzhou P. R. China;</p> <p>Department of PharmacyThe First Affiliated Hospital of Zhengzhou UniversityZhengzhou P. R. China;</p> <p>Department of PharmacyThe First Affiliated Hospital of Zhengzhou UniversityZhengzhou P. R. China;</p> <p>Department of PharmacyThe First Affiliated Hospital of Zhengzhou UniversityZhengzhou P. R. China;</p> <p>Department of PharmacyThe First Affiliated Hospital of Zhengzhou UniversityZhengzhou P. R. China;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/159.html" title="化学">化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=qualitative analysis&option=203" rel="nofollow">qualitative analysis;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=quantitative determination&option=203" rel="nofollow">quantitative determination;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=traditional Chinese medicine&option=203" rel="nofollow">traditional Chinese medicine;</a> </p> <div class="translation"> 机译：定性分析;定量测定;中医; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704025846937.html">Qualitative and quantitative determination of YiXinShu Tablet using ultra high performance liquid chromatography with Q Exactive hybrid quadrupole orbitrap high‐resolution accurate mass spectrometry</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sun Zhi&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Sun Zhi,</a> <a 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