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STRUCTURAL AND MAGNETIC PROPERTIES OF Mg-Co FERRITE NANOPARTICLES

机译:Mg-Co铁氧体纳米粒子的结构和磁性

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摘要

A series of magnesium-substituted cobalt ferrite nanoparticles Co1-xMgxFe2O4 (0.0 = x = 1.0, step 0.2), have been synthesized using sol-gel auto-combustion method. The powders calcined at 600, 700, and 800 degrees C for 3h Various characterization methods were used to investigate the prepared powders such as X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), and vibrating sample magnetometer (VSM). The XRD patterns of the synthesized samples confirm the formation of single phase spinal structured nanoparticles. FE-SEM image results show some agglomerated of spherical and polyhedral shape morphology. Moreover, the average crystallite size was found to be ranging from (55.146-68.434nm). Saturation magnetization (M-s), remanent magnetization (M-r), and coercivity (H-c) decreases with increase in Mg substitution as indicated by VSM at room temperature. Both the structural and magnetic properties of Mg-Co ferrite nanoparticles depend upon Mg2+ ions substitution.
机译:使用溶胶 - 凝胶自燃方法合成了一系列镁取代的钴铁氧体纳米颗粒CO1-XMGXFE2O4(0.0.0& = 1.0,步骤0.2)。在600,700和800℃下煅烧的粉末各种表征方法用于研究制备的粉末,例如X射线衍射(XRD),场发射扫描电子显微镜(Fe-SEM)和振动样品磁力计( VSM)。合成样品的XRD图案证实了单相脊髓结构纳米颗粒的形成。 Fe-SEM图像结果显示了一些球形和多面体形态形态的凝聚。此外,发现平均微晶尺寸范围为(55.146-68.434nm)。饱和磁化强度(M-S),剩余磁化(M-R)和矫顽力(H-C)随着在室温下的VSM指示而增加的Mg替换量增加。 Mg-Co铁氧体纳米颗粒的结构和磁性均取决于Mg2 +离子取代。

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