Development and validation of a sensitive UPLC–MS/MS instrumentation and alkaline nitrobenzene oxidation method for the determination of lignin monomers in wheat straw

Mengjing Zheng; Shubo Gu; Jin Chen; Yongli Luo; Wenqian Li; Jun Ni; Yong Li; Zhenlin Wang

首页> 外文期刊>Journal of chromatography, B. Analytical technologies in the biomedical and life sciences >Development and validation of a sensitive UPLC–MS/MS instrumentation and alkaline nitrobenzene oxidation method for the determination of lignin monomers in wheat straw

【24h】

Development and validation of a sensitive UPLC–MS/MS instrumentation and alkaline nitrobenzene oxidation method for the determination of lignin monomers in wheat straw

机译：敏感UPLC-MS / MS仪表和碱性硝基苯氧化方法的开发和验证，用于测定小麦秸秆中木质素单体的氧化方法

获取原文

获取原文并翻译 | 示例

获取外文期刊封面封底 >>

开具论文收录证明 >>

文献代查 >>

团队文献服务 >>

页面导航

摘要
著录项
引文网络
相似文献
相关主题

摘要

Highlights

? Appling for the method of UPLC–MS/MS to determine the three lignin monomers in wheat straw.

? We have optimized the conditions of chromatography system and MS.

? Realized high-throughput due to improvement of the nitrobenzene oxidation method.

Abstract

A method to determine the lignin monomers (p-hydroxybenzaldehyde, vanillin and syringaldehyde) in plant cell wall of wheat internode was developed and validated using a high-throughput nitrobenzene oxidation step and ultra performance liquid chromatography tandem mass spectrometry (UPLC–MS/MS) for quantification. UPLC analyses were carried out using an reversed phase C

机译：<！[cdata [

突出显示

？

？我们已经优化了条件色谱系统和MS。

？由于硝基苯氧化方法的改进而实现的高吞吐量。 < / ce：abstract-sec> 抽象

p - 羟基苯甲醛，香草醛和syringaldede）的方法，并使用高通量硝基苯氧化步骤和验证超高效液相色谱串联质谱（UPLC-MS / MS）进行量化。使用反相C

著录项

来源
《Journal of chromatography, B. Analytical technologies in the biomedical and life sciences》 |2017年第2017期|共7页
作者
Mengjing Zheng; Shubo Gu; Jin Chen; Yongli Luo; Wenqian Li; Jun Ni; Yong Li; Zhenlin Wang;
展开▼
作者单位

State Key Laboratory of Crop Biology Ministry of Science and Technology Shandong Agricultural University;

State Key Laboratory of Crop Biology Ministry of Science and Technology Shandong Agricultural University;

State Key Laboratory of Crop Biology Ministry of Science and Technology Shandong Agricultural University;

State Key Laboratory of Crop Biology Ministry of Science and Technology Shandong Agricultural University;

State Key Laboratory of Crop Biology Ministry of Science and Technology Shandong Agricultural University;

State Key Laboratory of Crop Biology Ministry of Science and Technology Shandong Agricultural University;

State Key Laboratory of Crop Biology Ministry of Science and Technology Shandong Agricultural University;

State Key Laboratory of Crop Biology Ministry of Science and Technology Shandong Agricultural University;

展开▼
收录信息
原文格式 PDF
正文语种 eng
中图分类生物化学技术;
关键词
UPLC–MS/MS; Nitrobenzene oxidation; Lignin monomer; Wheat straw;

机译：UPLC-MS / MS;硝基苯氧化;木质素单体;小麦秸秆;

相似文献

外文文献
中文文献
专利

1. Development and validation of a sensitive UPLC–MS/MS instrumentation and alkaline nitrobenzene oxidation method for the determination of lignin monomers in wheat straw [J] . Mengjing Zheng, Shubo Gu, Jin Chen, Journal of chromatography, B. Analytical technologies in the biomedical and life sciences . 2017,第期

机译：敏感UPLC-MS / MS仪表和碱性硝基苯氧化方法的开发和验证，用于测定小麦秸秆中木质素单体的氧化方法
2. Development and validation of a sensitive and fast UPLC-MS/MS method for simultaneous determination of seven bioactive compounds in rat plasma after oral administration of Guizhi-gancao decoction [J] . Ji Bin, Zhuo Limeng, Yang Bin, Journal of Pharmaceutical and Biomedical Analysis: An International Journal on All Drug-Related Topics in Pharmaceutical, Biomedical and Clinical Analysis . 2017,第期

机译：桂花 - 甘草口服施氮后大鼠血浆同时测定七种生物活性化合物的敏感和快速UPLC-MS / MS方法的开发和验证
3. Development and validation of sensitive and rapid UPLC-MS/MS method for quantitative determination of daclatasvir in human plasma: Application to a bioequivalence study [J] . Rezk Mamdouh R., Bendas Ehab R., Basalious Emad B., Journal of Pharmaceutical and Biomedical Analysis: An International Journal on All Drug-Related Topics in Pharmaceutical, Biomedical and Clinical Analysis . 2016,第Null期

机译：灵敏快速的UPLC-MS / MS方法的开发和验证，用于定量测定人血浆中的达卡他韦：在生物等效性研究中的应用
4. A Simple, Selective and Highly Sensitive UPLC-MS/MS Method for Determination of Mometasone Furoate in Human Plasma [C] . Hao Li, Huafang Jiang, Ling Zhou, ASMS Conference on Mass Spectrometry and Allied Topics . 2014

机译：一种简单，选择性和高度敏感的UPLC-MS / MS方法，用于测定人血浆中的米多酮呋喃
5. Development and validation of UPLC/MS/MS methods for quantification of gangliosides in the clinical study of ganglioside GM3 synthase deficiency. [D] . Huang, Qianyang. 2016

机译：神经节苷脂GM3合酶缺乏症临床研究中用于定量神经节苷脂的UPLC / MS / MS方法的开发和验证。
6. Development and Validation of a UPLC-MS/MS and UPLC-HR-MS Method for the Determination of Fumonisin B1 and Its Hydrolysed Metabolites and Fumonisin B2 in Broiler Chicken Plasma [O] . Siegrid De Baere, Siska Croubels, Barbara Novak, 2018

机译：建立UPLC-MS / MS和UPLC-HR-MS方法测定肉鸡鸡肉中伏马毒素B1及其水解产物和伏马毒素B2的建立和验证
7. Validação de método multirresíduo para determinação de pesticidas em alimentos empregando QuEChERS E UPLC-MS/MS Multiresidue method validation for determination of pesticides in food using QuEChERS and UPLC-MS/MS [O] . Sonia C. N. Queiroz, Vera L. Ferracini, Maria A. Rosa 2012

机译：使用QuEChERS和UPLC-MS / MS验证食品中农药残留的多残留方法验证通过QuEChERS和UPLC-MS / MS验证食品中农药残留的多残留方法验证

Development and validation of a sensitive UPLC–MS/MS instrumentation and alkaline nitrobenzene oxidation method for the determination of lignin monomers in wheat straw

摘要

著录项

引文网络

相似文献

相关主题

期刊订阅