Study on the Crystallization Rates of β‐ and ?‐form HNIW in in‐situ Raman Spectroscopy and FBRM

Yang Hee‐og; Kim Jun‐Hyung; Kim Kwang‐Joo

摘要

Abstract >Kinetics of anti‐solvent crystallization of HNIW polymorphs were studied using in?situ Raman spectroscopy and focused beam reflectance measurement (FBRM). Crystal polymorphs and supersaturation were monitored in?situ by Raman spectroscopy. Crystal counts and crystal size were monitored by FBRM during anti‐solvent crystallization. The addition rate of the anti‐solvent affected the polymorph transformation, the first polymorph of the crystals, and supersaturation. At a wide range of addition rate, the unstable form, β‐form, was detected and then transformed to the stable form, ?‐form. By controlling the concentration and rate of addition, the stable form, ?‐form was only nucleated and grown without transformation. This process depended on the supersaturation and affected polymorphic transformation, concentration, nucleation rate, and growth rate, which were simultaneously monitored by Raman spectroscopy and FBRM. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> 研究了HNIW多晶型物的抗溶剂结晶的动力学，使用？原位拉曼光谱和聚焦光束反射测量（FBRM）。通过拉曼光谱法监测晶体多晶型物和过饱和。通过FBRM在抗溶剂结晶期间监测晶体计数和晶体尺寸。抗溶剂的添加速率影响了多晶型转化，晶体的第一多晶型物和过饱和。在宽范围的添加速率下，检测不稳定形式，β-形式，然后转化为稳定的形式，α-Form。通过控制添加的浓度和速率，稳定的形式，β--form仅在没有转化的情况下成核并生长。该方法取决于过饱和和影响的多晶晶晶型转化，浓度，成核速率和生长速率，通过拉曼光谱和FBRM同时监测。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-29946/'>《Propellants, Explosives, Pyrotechnics》</a> <b style="margin: 0 2px;">|</b><span>2020年第3期</span><b style="margin: 0 2px;">|</b><span>共9页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Yang Hee‐og&option=202" target="_blank" rel="nofollow">Yang Hee‐og;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kim Jun‐Hyung&option=202" target="_blank" rel="nofollow">Kim Jun‐Hyung;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kim Kwang‐Joo&option=202" target="_blank" rel="nofollow">Kim Kwang‐Joo;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Biological and Chemical EngineeringHanbat National University125 Dongseodaero Yuseong-gu Daejeon 305-718 Korea;</p> <p>Agency for Defense Development462 Jochiwon-gil Yuseong-gu Daejeon 305-150 Republic of Korea;</p> <p>Department of Biological and Chemical EngineeringHanbat National University125 Dongseodaero Yuseong-gu Daejeon 305-718 Korea;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1837.html" title="爆炸物工业、火柴工业">爆炸物工业、火柴工业;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=CL-20&option=203" rel="nofollow">CL-20;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=FBRM&option=203" rel="nofollow">FBRM;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Raman Spectroscopy&option=203" rel="nofollow">Raman Spectroscopy;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Anti-Solvent Crystallization&option=203" rel="nofollow">Anti-Solvent Crystallization;</a> </p> <div class="translation"> 机译：CL-20;FBRM;拉曼光谱;抗溶剂结晶; 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