Catalytic Cycloaminomethylation of Aminobenzamides with 1,3-Bis[dimethylamino(methoxy)methyl]thiourea

Khairullina R. R.; Tyumkina T. V.; Geniyatova A. R.; Abdullin M. F.; Ibragimov A. G.

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Catalytic Cycloaminomethylation of Aminobenzamides with 1,3-Bis[dimethylamino(methoxy)methyl]thiourea

机译：用1,3-双α氨基苯甲酰胺催化环酰胺甲基化硫脲硫脲

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摘要

Efficient methods of the synthesis of cyclophanes containing the thiourea moiety via the reaction of o-, m-, and p-aminobenzamides with 1,3-bis(dimethylaminomethyl)thiourea or 1,3-bis(methoxymethyl)thiourea using NiCl(2)6H(2)O and SmCl(3)6H(2)O as catalysts have been developed.

机译：使用NiCl（2）的1,3-双（二甲基氨基甲基）硫脲或1,3-双（甲氧基甲基）硫脲（2），通过用O-，M-和氨基苯甲酰胺的反应合成含有硫脲部分的环烷基酚的环烷的合成方法已经开发了催化剂的6H（2）o和Smcl（3）6（2）o。

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《Russian Journal of General Chemistry》 |2019年第3期|共7页
作者
Khairullina R. R.; Tyumkina T. V.; Geniyatova A. R.; Abdullin M. F.; Ibragimov A. G.;
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作者单位

Russian Acad Sci Inst Petrochem &

Catalysis Pr Oktyabrya 141 Ufa 450075 Russia;

Russian Acad Sci Inst Petrochem &

Catalysis Pr Oktyabrya 141 Ufa 450075 Russia;

Russian Acad Sci Inst Petrochem &

Catalysis Pr Oktyabrya 141 Ufa 450075 Russia;

Russian Acad Sci Ufa Inst Chem Pr Oktyabrya 71 Ufa 450054 Russia;

Russian Acad Sci Inst Petrochem &

Catalysis Pr Oktyabrya 141 Ufa 450075 Russia;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
cycloaminomethylation; aminobenzamides; bis(N; N-dimethylamino)methane; thiourea; cyclophanes;

机译：环酰胺甲基化;氨基苯甲酰胺;双（n;n-二甲基氨基）甲烷;硫脲;环野;

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专利

1. Catalytic Cycloaminomethylation of Aminobenzamides with 1,3-Bis[dimethylamino(methoxy)methyl]thiourea [J] . Khairullina R. R., Tyumkina T. V., Geniyatova A. R., Russian Journal of General Chemistry . 2019,第3期

机译：用1,3-双α氨基苯甲酰胺催化环酰胺甲基化硫脲硫脲
2. Catalytic Aminomethylation of Aminobenzamides with Bis(N,N-dimethylamino)methane and Carbamides [J] . Khairullina R. R., Tyumkina T. V., Geniyatova A. R., Russian Journal of General Chemistry . 2019,第2期

机译：用双（n，N-二甲基氨基）甲烷和氨基甲酰胺的氨基苯甲酰胺催化氨基甲基化
3. Synthesis of 2-aryl-3-methylbenzo[g]indoles from 2-(arylethynyl)-1,8-bis(dimethylamino)naphthalenes: new examples of [1,3]-migration involving N-methyl group [J] . Filatova Ekaterina A., Gulevskaya Anna V., Pozharskii Alexander F. Chemistry of heterocyclic compounds . 2018,第1期

机译：来自2-（芳基乙炔基）-1,8-双（二甲基氨基）萘的2-芳基-3-甲基甲基苯基吲哚的合成：[1,3] - 涉及N-甲基的新实例
4. Bis(2-chloroethyl) ether-1,3-bis3-(Dimethylamino)propylurea copolymer -Chitosan-Poly(acrylamide-co-diallyldimethylammonium chloride) blends as membranes For Alkaline Anion-exchange Membranes [C] . Bei Ao, Yanan Wei, Jinli Qiao Electrochemical Society, Meeting . 2017

机译：双（2-氯乙基）醚-1,3-双3-（二甲基氨基）丙基脲共聚物 - 硫酸烷聚（丙烯酰胺 - 共二甲基氯化铵）混合为碱性阴离子交换膜的膜
5. Substitution chemistry of ruthenium clusters with the diphosphine ligands: 4,5-bis(diphenylphosphino)-4-cyclo-penten-1,3-dione (BPCD), (Z)-Ph(2)PCH=CHPPh(2) and 3,4-bis(diphenylphosphino)-5-methoxy-2(5H)-furanone (BMF). [D] . Shen, Huanfeng. 1997

机译：具有二膦配体的钌簇的取代化学：4,5-双（二苯基膦基）-4-环戊烯-1,3-二酮（BPCD），（Z）-Ph（2）PCH = CHPPh（2）和3 ，4-双（二苯基膦基）-5-甲氧基-2（5H）-呋喃酮（BMF）。
6. 2-[4,5-Bis(ethylsulfanyl)-1,3-dithiol-2-ylidene]-5-(4-methoxyphenyl)-5H-1,3-dithiolo[4,5-c]pyrrole [O] . Feng-Shou Leng, Bao Li, Bing-Zhu Yin, 2016

机译：2- [4,5-双（乙基硫烷基）-1,3-二硫醇-2-基亚烷基] -5-（4-甲氧基基）-5H-1,3-二硫代[4,5-c]吡咯
7. Bis(1,3-benzothiazole-2-thiolato)[(Z)-methyl 2-(2-amino-1,3-thiazol-4-yl)-2-(methoxyimino)acetate]nickel(II) [O] . Khan, Islam Ullah, Şahin, Onur, Jillani, Shehzada Muhammad Sajid, 2010

机译：双（1,3-苯并噻唑-2-硫醇）[（Z）-2-（2-氨基-1,3-噻唑-4-基）-2-（甲氧基亚氨基）乙酸甲酯]镍（II）
8. Summary of Health Effects Alleged by a Property Owner Following Potential Inhalation Exposure to a Chemical Mixture Manufactured or Processed by the Company with 2-Propanol, 1-(bis(3-(dimethylamino) propyl)amino); 1,3-Propanediamine, N1-(3-(dimethylamino)propyl)-N1, N3, N3-trimethyl; 1H-Imidazole, 1,2-dimethyl; 1,2-Dichloroethylene; 1,1,1,3,3-Pentafluoropropane; 2-Butoxyethanol. [R] . 2013

机译：在公司制造或加工的化学混合物中，使用2-丙醇，1-（双（3-（二甲基氨基）丙基）氨基）吸收潜在吸入后财产所有者所指称的健康影响摘要; 1,3-丙二胺，N1-（3-（二甲基氨基）丙基）-N1，N3，N3-三甲基; 1H-咪唑，1,2-二甲基; 1,2-二氯乙烯; 1,1,1,3,3-五氟丙烷; 2-丁氧基乙醇。

Catalytic Cycloaminomethylation of Aminobenzamides with 1,3-Bis[dimethylamino(methoxy)methyl]thiourea

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