Catalytic Aminomethylation of Aminobenzamides with Bis(N,N-dimethylamino)methane and Carbamides

Khairullina R. R.; Tyumkina T. V.; Geniyatova A. R.; Mullagildina F. K.; Ibragimov A. G.

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Catalytic Aminomethylation of Aminobenzamides with Bis(N,N-dimethylamino)methane and Carbamides

机译：用双（n，N-二甲基氨基）甲烷和氨基甲酰胺的氨基苯甲酰胺催化氨基甲基化

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摘要

An effective method was developed for the synthesis of acyclic aniline derivatives bearing carbamide fragments by the reaction of carbamides with ortho-, meta-, and para-aminobenzamides and bis(N,N-dimethylamino) methane in the presence of NiCl(2)6H(2)O and SmCl(3)6H(2)O as catalysts.

机译：开发有效的方法，用于通过氨基甲酰（2）6小时在存在下的氨基甲酰（2）6小时内通过氨基甲酰胺与氨基甲酰胺反应合成携带氨基甲酰胺片段的无环苯胺衍生物。（2）o和smcl（3）6h（2）o作为催化剂。

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来源
《Russian Journal of General Chemistry》 |2019年第2期|共8页
作者
Khairullina R. R.; Tyumkina T. V.; Geniyatova A. R.; Mullagildina F. K.; Ibragimov A. G.;
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作者单位

Russian Acad Sci Inst Petrochem &

Catalysis Pr Oktyabrya 141 Ufa 450075 Russia;

Russian Acad Sci Inst Petrochem &

Catalysis Pr Oktyabrya 141 Ufa 450075 Russia;

Russian Acad Sci Inst Petrochem &

Catalysis Pr Oktyabrya 141 Ufa 450075 Russia;

Russian Acad Sci Inst Petrochem &

Catalysis Pr Oktyabrya 141 Ufa 450075 Russia;

Russian Acad Sci Inst Petrochem &

Catalysis Pr Oktyabrya 141 Ufa 450075 Russia;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
aminomethylation; aminobenzamides; bis(N; N-dimethylamino)methane; carbamides;

机译：氨基甲基化;氨基苯甲酰胺;双（n;N-二甲基氨基）甲烷;氨基甲酰胺;

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专利

1. Catalytic Aminomethylation of Aminobenzamides with Bis(N,N-dimethylamino)methane and Carbamides [J] . Khairullina R. R., Tyumkina T. V., Geniyatova A. R., Russian Journal of General Chemistry . 2019,第2期

机译：用双（n，N-二甲基氨基）甲烷和氨基甲酰胺的氨基苯甲酰胺催化氨基甲基化
2. Preparation and Characterization of a Heterogeneous Catalyst from Water Hyacinth (Eichhornia crassipes): Catalytic Application in the Synthesis of bis(indolyl)methanes and bis(pyrrolyl) methanes Under Solvent Free Condition [J] . Anjumani Talukdar, Dibakar Chandra Deka Current Catalysis . 2016,第1期

机译：水葫芦（Eichhornia crassipes）的多相催化剂的制备和表征：无溶剂条件下催化合成双（吲哚基）甲烷和双（吡咯基）甲烷
3. Poly(N,N'-dichloro-N-ethyl-benzene-1, 3-disulfonamide) and N,N,N',N'-tetrachlorobenzene-1,3-disulfonamide as novel catalytic reagents for synthesis of bis-indolyl, tris-indolyl, di(bis-indolyl), tri(bis-indolyl) and tetra(bis-indolyl)methanes under solid-state, solvent and water conditions [J] . Hojat Veisi, Ramin Ghorbani-vaghei Journal of the Brazilian Chemical Society . 2010,第2期

机译：聚（N，N'-二氯-N-乙基苯-1,3-二磺酰胺）和N，N，N'，N'-四氯苯-1,3-二磺酰胺为合成双吲哚基的新型催化试剂，固态，溶剂和水条件下的三吲哚基甲烷，二（双吲哚基），三（双吲哚基）和四（双吲哚基）甲烷
4. Catalytic Decomposition of Methane: Effect of Various Factors on Catalytic Properties [C] . Hyun Chang Shin, Hyun Jung Kim, Dong Shin Yun, Eco-Materials Processing and Design VIII; Materials Science Forum; vols.544-545 . 2007

机译：甲烷的催化分解：各种因素对催化性能的影响
5. Toward a catalytic system cycle for the hydroxylation of methane: Oxy-functionalization of electron rich M-methane bonds [D] . Conley, Brian Lee 2008

机译：迈向甲烷羟基化的催化系统循环：富电子的M-甲烷键的氧化官能化
6. Development of an imidazole salt catalytic system for the preparation of bis(indolyl)methanes and bis(naphthyl)methane [O] . Xu Wang, Courtney C. Aldrich 2012

机译：开发用于制备双（吲哚基）甲烷和双（萘基）甲烷的咪唑盐催化系统
7. Poly(N,N'-dichloro-N-ethyl-benzene-1, 3-disulfonamide) and N,N,N',N'-tetrachlorobenzene-1,3-disulfonamide as novel catalytic reagents for synthesis of bis-indolyl, tris-indolyl, di(bis-indolyl), tri(bis-indolyl) and tetra(bis-indolyl)methanes under solid-state, solvent and water conditions [O] . Ramin Ghorbani-Vaghei, Hojat Veisi 2010

机译：聚（N，N'-二氯-N-乙基 - 苯-1,3-二硫磺酰胺）和N，N，N'，N'-四氯苯-1,3-二磺酰胺作为新型催化试剂，用于合成双吲哚（BIS-Indolyl），在固态，溶剂和水条件下，Tris-Indolyl，DI（双吲哚基），三（双吲哚基）和四（双吲哚基）甲烷

Catalytic Aminomethylation of Aminobenzamides with Bis(N,N-dimethylamino)methane and Carbamides

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