Sustainable and Site‐Selective C?H Sulfenylation of Aromatic Compounds with Thiol using Catalytic Graphene Oxide and NaI

Choudhury Prasun; Roy Babli; Basu Basudeb

摘要

Abstract > Graphene oxide (GO) in combination with NaI is used as the catalytic system for site‐selective C?H sulfenylation of 1 H ‐indole, 2‐naphthol, resorcinol and 2‐naphthylamines with thiols. The reaction is usually achieved in the presence of metal catalysts as well as under metal‐free conditions using iodine and a strong oxidizing agent. The present protocol avoids the use of any metal catalysts, strong oxidizing agents and the use of thiols instead of other sulfur‐based reagents making it atom‐economic and environmentally benign. Broader tolerance to functional groups has been tested and a plausible mechanism is proposed. The recovered GO can be recycled without significant loss in catalytic activity up to four runs. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract XMLNS =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> >石墨烯氧化物（GO）与Nai组合用作现场选择性C 2的催化系统1〜11℃，2-萘酚，间苯二酚和2-萘胺与硫醇。通常在金属催化剂存在下以及使用碘和强氧化剂的无金属条件下进行反应。本方案避免了使用任何金属催化剂，强氧化剂和硫醇的使用而不是其他硫的试剂，使其成为原子经济和环境良性。已经测试了更广泛的功能组的耐受性，并提出了一种合理的机制。可以回收回收的GO再循环，在催化活性的显着损失，高达四次运行。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-19765/'>《Asian Journal of Organic Chemistry》</a> <b style="margin: 0 2px;">|</b><span>2017年第11期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Choudhury Prasun&option=202" target="_blank" rel="nofollow">Choudhury Prasun;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Roy Babli&option=202" target="_blank" rel="nofollow">Roy Babli;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Basu Basudeb&option=202" target="_blank" rel="nofollow">Basu Basudeb;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of ChemistryNorth Bengal UniversityDarjeeling 734013 India;</p> <p>Department of ChemistryNorth Bengal UniversityDarjeeling 734013 India;</p> <p>Department of ChemistryNorth Bengal UniversityDarjeeling 734013 India;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1184.html" title="有机化学">有机化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=graphene oxide&option=203" rel="nofollow">graphene oxide;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=indoles&option=203" rel="nofollow">indoles;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=naphthols&option=203" rel="nofollow">naphthols;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=naphthylamines&option=203" rel="nofollow">naphthylamines;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=resorcinol&option=203" rel="nofollow">resorcinol;</a> </p> <div class="translation"> 机译：石墨烯氧化物;吲哚;萘酚;萘胺;间苯二酚; </div> </li> </ul> </div> </div> <div class="literature cardcommon" id="literaturereference" style="display:none"> <div class="similarity "> <h3 class="all_title" id="enpatent111">引文网络</h3> <div class="referencetab clearfix"> <ul id="referencedaohang"> <li dataid="referenceul">参考文献</li> <li dataid="citationul">引证文献</li> <li dataid="commonreferenceul">共引文献</li> <li dataid="commoncitationul">同被引文献</li> <li dataid="tworeferenceul">二级参考文献</li> <li dataid="twocitationul">二级引证文献</li> </ul> </div> <div class="reference_details" id="referenceList"> <ul id="referenceul"></ul> <ul id="citationul"></ul> <ul id="commonreferenceul"></ul> <ul id="commoncitationul"></ul> <ul id="tworeferenceul"></ul> <ul id="twocitationul"></ul> </div> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022773969.html">Sustainable and Site‐Selective C?H Sulfenylation of Aromatic Compounds with Thiol using Catalytic Graphene Oxide and NaI</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Choudhury Prasun&option=202" target="_blank" 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target="_blank" rel="nofollow" class="tuijian_authcolor"> . 现代化工 </a> </span> <span> . 2006</span><span>,第z1期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_detail_thesis/0201297268603.html">相转移催化环加成反应合成1-芳磺酰基-2-苯甲酰基环丙烷系列化合物(Ⅱ)</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘长畿&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 刘长畿</a> <span> <a href="/journal-cn-57029/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 化学试剂 </a> </span> <span> . 1996</span><span>,第5期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-59545_thesis/020222595692.html">镍铁复合氧化物催化水合肼氢转移还原芳硝基化合物的研究</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=石奇勋&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 石奇勋</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吕荣文&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,吕荣文</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=邹伟&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,邹伟</a> <span> <a href="/conference-cn-59545/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第十一届全国青年催化学术会议 </a> <span> <span> . 2007</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314705441.html">邻硝基促进的选择性去酰基化和去磺酰化反应与碘、氧化叔胺双重催化的过氧化氢氧化苄醇的绿色新反应初步研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=纪秀杰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 纪秀杰</a> <span> . 2006</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120104459019.html">芳族化合物的酰化或磺酰化方法</a> <b>[P]</b> . <span> 中国专利： CN1249737A </span> <span> . 2000-04-05</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120113250736.html">通过保存甲基芳族化合物氢解乙基芳族化合物的选择性催化剂</a> <b>[P]</b> . <span> 中国专利： CN113302264A </span> <span> . 2021-08-24</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130446938786.html">Method for catalytic and selective oxidation of aromatic compounds</a> <b>[P]</b> . <span> 外国专利：  US6365762B1 </span> <span> . 2002-04-02</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：催化和选择性氧化芳族化合物的方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130450369843.html">METHOD FOR CATALYTIC AND SELECTIVE OXIDATION OF AROMATIC COMPOUNDS</a> <b>[P]</b> . <span> 外国专利：  EP0975559A1 </span> <span> . 2000-02-02</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：芳香化合物的催化和选择性氧化的方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130452359733.html">Method for catalytic and selective oxidation of aromatic compounds</a> <b>[P]</b> . <span> 外国专利：  AU7213198A </span> <span> . 1998-11-13</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：催化和选择性氧化芳族化合物的方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" 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