High‐performance liquid chromatographic enantioseparation of NN ‐aryl‐thioureidoalkylphosphonates and thiourylenedi(alkylphosphonates) on polysaccharide‐based chiral stationary phases

机译： n-in-in-inhiouroido烷基膦酸盐和硫胺（烷基膦酸盐）对基于多糖的手性静脉阶段的高性能液相色谱映像分析

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Abstract > The first successful enantioseparation of representative <fi>O,O</fi> ‐diphenyl‐ <fi>N</fi> ‐arylthioureidoalkylphosphonates, (±)‐Ptc‐Val P (OPh) <sub>2</sub> & (±)‐Ptc‐Leu P (OPh) <sub>2</sub> and thiourylenedi(isobutyl phosphonate), Tcm[Val P (OPh) <sub>2</sub> ] <sub>2</sub> on analytical and semipreparative scale was achieved by high‐performance liquid chromatography using polysaccharide‐based chiral stationary phases (CPs). Atc‐AA P (OPh) <sub>2</sub> was obtained using modified tricomponent condensations of the corresponding aldehydes, <fi>N</fi> ‐arylthiourea and triphenyl phosphite whereas Tcm[Val P (OPh) <sub>2</sub> ] <sub>2</sub> by the condensations of aldehydes, thiourea, and triphenyl phosphite. The prepared, racemic (±)‐Atc‐AA P (OPh) <sub>2</sub> [(±)‐Ptc‐Val P (OPh) <sub>2</sub> , (±)‐Ptc‐Leu P (OPh) <sub>2</sub> , (±)‐Ptc‐Pgly P (OPh) <sub>2</sub> and (±)‐Ntc‐Pgly P (OPh) <sub>2</sub> ] and racemic (±)‐Tcm[AA P (OPh) <sub>2</sub> ] <sub>2</sub> [(±)‐Tcm[Nva P (OPh) <sub>2</sub> ] <sub>2</sub> & (±)‐Tcm[Val P (OPh) <sub>2</sub> ] <sub>2</sub> ] were adequately characte </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >代表的第一个成功的阐述<fi> o，o </ fi> -diphenyl- <fi> n </ fi> - 硫代萘烷基膦酸盐，（±）-ptc-val p </ sup>（OPH）<sub> 2 </ sub>＆amp; （±）-ptC-Leu p </ sup>（OPH）<sub> 2 </ sub>和硫硝丁烯（异丁基膦酸盐），tcm [val p </ sup>（oph）<sub>通过使用基于多糖的手性固定阶段（CPS）的高性能液相色谱法实现了分析和半乙醛的2 </ sub>] <sub> 2 </ sub>。使用相应的醛的改性的三分组分缩合获得ATC-AA p </ sup>（OPH）<sub> 2 </ sub>，<fi> n </ fi> - 亚芳硫脲和三苯基亚磷矿，而TCM [val通过醛，硫脲和三苯基亚磷矿的缩合来 p </ sup>（OPH）<sub> 2 </ sub>] <sub> 2 </ sub>。制备的外消旋（±）-ATC-AA p </ sup>（OPH）<sub> 2 </ sub> [（±）-ptc-val p </ sup>（oph）< Sub> 2 </ sub>，（±）-ptc-Leu p </ sup>（OPH）<sub> 2 </ sub>，（±）-ptc-pgly p </ sup> （OPH）<sub> 2 </ sub>和（±）-ntc-pgly p </ sup>（OPH）<sub> 2 </ sub>]和外消旋（±）-tcm [aa <sup > P </ sup>（OPH）<sub> 2 </ sub>] <sub> 2 </ sub> [（±）-tcm [nva p </ sup>（oph）<sub> 2 < / sub>] <sub> 2 </ sub>＆amp; （±）-tcm [val p </ sup>（OPH）<sub> 2 </ sub>] <sub> 2 </ sub>]是充分的characte </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16290/'>《Chirality: The pharmacological, biological, and chemical consequences of molecular asymmetry》</a> <b style="margin: 0 2px;">|</b><span>2018年第2期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Drabowicz Józef&option=202" target="_blank" rel="nofollow">Drabowicz Józef;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kudzin Marcin H.&option=202" target="_blank" rel="nofollow">Kudzin Marcin H.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kudzin Zbigniew H.&option=202" target="_blank" rel="nofollow">Kudzin Zbigniew H.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Pokora‐Sobczak Patrycja&option=202" target="_blank" rel="nofollow">Pokora‐Sobczak Patrycja;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Centre of Molecular and Macromolecular StudiesPolish Academy of SciencesWarsaw Poland;</p> <p>Textile Research InstituteLodz Poland;</p> <p>Faculty of ChemistryUniversity of LodzLodz Poland;</p> <p>Centre of Molecular and Macromolecular StudiesPolish Academy of SciencesWarsaw Poland;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/4812.html" title="结构化学">结构化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=chiral HPLC&option=203" rel="nofollow">chiral HPLC;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=enantiomers&option=203" rel="nofollow">enantiomers;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=meso compounds&option=203" rel="nofollow">meso compounds;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=N ‐arylthioureidoalkylphosphonates&option=203" rel="nofollow">N ‐arylthioureidoalkylphosphonates;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=thioureas&option=203" rel="nofollow">thioureas;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=thiourylenedi(alkylphosphonates)&option=203" rel="nofollow">thiourylenedi(alkylphosphonates);</a> </p> <div class="translation"> 机译：手性HPLC;对映异构体;中索化合物;N-芳硫代烷烷基膦酸盐;硫酸;硫酸丁苯（烷基膦酸盐）; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022113452.html">High‐performance liquid chromatographic enantioseparation of <fi >N</fi>N ‐aryl‐thioureidoalkylphosphonates and thiourylenedi(alkylphosphonates) on polysaccharide‐based chiral stationary phases</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Drabowicz Józef&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Drabowicz Józef,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kudzin Marcin H.&option=202" target="_blank" rel="nofollow" class="tuijian_auth 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<span>机译：基于异孔的β-氨基内酯和β-氨基酰胺类似物对多糖的手性固定阶段的高效液相色谱映像分析，其关注对映体洗脱序列的变化</span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/academic-conference-foreign_meeting-222126_thesis/020515368603.html">Chromatographic chiral separation on chiral stationary phase by HPLC: Cellulose 4-methylbenzoate beads as chiral stationary phase for chiral separation of some racemates by high performance liquid chromatography</a> <b>[C]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Han Xiaoqian&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Han Xiaoqian,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Dabing&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Zhang Dabing,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Liu Wanliang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Liu Wanliang,</a> <a href="/conference-foreign-222126/" target="_blank" rel="nofollow" class="tuijian_authcolor">2011 International Conference on Consumer Electronics, Communications and Networks .</a> <span>2011</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：HPLC在手性固定相上进行色谱手性分离：以4-甲基苯甲酸纤维素微珠为手性固定相，通过高效液相色谱手性分离某些外消旋体</span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-degree-foreign_mphd_thesis/02061477930.html">Development of a new polysaccharide-based chiral stationary phase for high-performance liquid chromatography.</a> <b>[D] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lynch, Jeffry James.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Lynch, Jeffry James. </a> <span>1994</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：新型基于多糖的高效液相色谱手性固定相的开发。</span> </p> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-journal-foreign-pmc_detail_thesis/040005868893.html">High-performance liquid chromatographic enantioseparation of Betti base analogs on a newly developed isopropyl carbamate-cyclofructan6-based (IP-CF6) chiral stationary phase</a> <b>[O] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ANITA ARANYI&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">ANITA ARANYI,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ISTVÁN ILISZ&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">ISTVÁN ILISZ,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ZOLTÁN PATAJ&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">ZOLTÁN PATAJ,</a> <span>-1</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：在新开发的异丙基氨基甲酸酯-ConcOfructan6（IP-CF6）手性固定阶段的高效液相色谱映像对β基碱基酶进行分析</span> </p> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/open-access_resources_thesis/0100016719754.html ">High-performance liquid chromatographic enantioseparation of unusual amino acid derivatives with axial chirality on polysaccharide-based chiral stationary phases</a> <b>[O] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=López-Ram-de-Víu, Pilar&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">López-Ram-de-Víu, Pilar,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gálvez, José A.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Gálvez, José A.,</a> <a 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tuijian_authcolor">,贺峥杰</a> <span> <a href="/journal-cn-26737/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 农药译丛 </a> </span> <span> . 1998</span><span>,第004期</span> </span> </div> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/academic-journal-cn_physical-testing-chemical-analysis-part-bchemical-analysis_thesis/0201212449477.html">柱前衍生-高效液相色谱法测定油田采出液中的烷基胺碳酸盐型表面活性剂</a> <b>[J]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=姚峰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 姚峰</a> <span> <a href="/journal-cn-7677/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 理化检验-化学分册 </a> </span> <span> . 2017</span><span>,第006期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-6670_thesis/020221732545.html">钯催化甲基苯基膦氢的不对称烷基化反应合成含膦手性中心化合物</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Chun&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . Li Chun</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李春&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,李春</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Weixun&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Li Weixun</a> <span> <a href="/conference-cn-6670/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第十七届全国金属有机化学学术讨论会 </a> <span> <span> . 2012</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020313129416.html">新型含膦β-二亚胺稀土金属配合物的合成及其在氢胺烷基化反应中的应用</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=高红杰&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 高红杰</a> <span> . 2018</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120109322.html">在三烷基胺或三烷基膦存在下对烷基或苄基氰衍生物烷基化的方法</a> <b>[P]</b> . <span> 中国专利： CN1119322C </span> <span> . 2003.08.27</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120104425556.html">在三烷基胺或三烷基膦存在下对烷基或苄基氰衍生物烷基化的方法</a> <b>[P]</b> . <span> 中国专利： CN1222505A </span> <span> . 1999-07-14</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130443849312.html">LC Liquid chromatographic ligand exchange chiral stationary phases chiral columns packed with the ligand exchange chiral stationary phases</a> <b>[P]</b> . <span> 外国专利：  KR20030077238A </span> <span> . 2003-10-01</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：LC液相色谱配体交换手性固定相填充有配体交换手性固定相的手性柱 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130439216655.html">LIQUID CHROMATOGRAPHIC CHIRAL CROWN ETHER-BASED STATIONARY PHASES WITH NOVEL DOUBLE TETHERING GROUPS AND THE CHIRAL COLUMNS</a> <b>[P]</b> . <span> 外国专利：  KR100516972B1 </span> <span> . 2005-09-26</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：液相色谱手性冠基于醚的固定相，具有两个双配位基团和手性柱 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130441595305.html">LIQUID CHROMATOGRAPHIC CHIRAL CROWN ETHER-BASED STATIONARY PHASES WITH NOVEL DOUBLE TETHERING GROUPS AND THE CHIRAL COLUMNS PACKED WITH THE SAME</a> <b>[P]</b> . <span> 外国专利：  KR20040090244A </span> <span> . 2004-10-22</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：液相色谱手性冠基于醚的固定相，具有两个双配位基团，并且手性柱具有相同的包装 </span> </p> </li> </ul> </div> </div> </div> <div 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