Pseudo porphyrinyl amino acids based on 1,3,5-triazine scaffold: new tools for the synthesis of peptidic porphyrins

Vincent Chaleix; Vincent Sol Pierre Krausz

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Pseudo porphyrinyl amino acids based on 1,3,5-triazine scaffold: new tools for the synthesis of peptidic porphyrins

机译：基于1,3,5-三嗪支架的伪卟啉氨基酸：肽卟啉合成的新工具

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摘要

Fmoc and Boc-protected pseudo meso-tetraarylporphyrin-based amino-acids were synthesized by sequential addition of nucleophiles to cyanuric chloride. These photosensitizers offer new scaffolds suitable for the generation of a large range of peptidic porphyrin derivatives designed for their use in photodynamic therapy.

机译：通过将亲核试剂顺序添加到氰尿酰氯中，合成了Fmoc和Boc保护的基于伪内消旋四芳基卟啉的氨基酸。这些光敏剂提供了新的支架，适用于生成大范围的肽卟啉衍生物，这些衍生物设计用于光动力疗法。

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2011年第23期|共3页
作者
Vincent Chaleix; Vincent Sol Pierre Krausz;
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正文语种 eng
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关键词
Porphyrin; 1; 3; 5-Triazine; PDT; Microwave; Synthesis;

机译：卟啉;1;3;5-三嗪;PDT;微波;合成;

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1. Pseudo porphyrinyl amino acids based on 1,3,5-triazine scaffold: new tools for the synthesis of peptidic porphyrins [J] . Vincent Chaleix, Vincent Sol Pierre Krausz Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2011,第23期

机译：基于1,3,5-三嗪支架的伪卟啉氨基酸：肽卟啉合成的新工具
2. Degradation of terbutylazine (2-chloro-4-ethylamino-6- terbutylamino-1,3,5-triazine), deisopropyl atrazine (2-amino-4-chloro-6-ethylamino-1,3,5-triazine), and chlorinated dimethoxy triazine (2-chloro-4,6-dimethoxy-1,3,5-triazine) by zero valent iron and [J] . T. Dombek, D. Davis, J. Stine, Environmental Pollution . 2004,第2期

机译：降解叔丁基嗪（2-氯-4-乙基氨基-6-叔丁基氨基-1,3,5-三嗪），去异丙基at去津（2-氨基-4-氯-6-乙基氨基-1,3,5-三嗪）和零价铁氯化氯化二甲氧基三嗪（2-氯-4,6-二甲氧基-1,3,5-三嗪）
3. Synthesis of ({8-[4,6-Bis-(bis-pyridin-2-ylmethyl-amino)-[1,3,5]triazine-2-ylamino]-octyl}—ethoxycarbonylmethyl-amino)-acetic acid ethyl ester [J] . Burkhard K?nig, Daniel Vomasta Molbank . 2007,第4期

机译：（{8- [4,6-双-（双吡啶-2-基甲基-氨基）-[1,3,5]三嗪-2-基氨基]-辛基}-乙氧基羰基甲基-氨基）-乙酸乙基的合成酯
4. Synthesis of potassium salts of 2,4-diamino(alkylamino)-6-dinitromethyl-1,3,5-triazine and 2-hydrazinyl-4-amino(alkylamino)-6-dinitromethyl-1,3,5-triazine [C] . Alexander A. Gidaspov, Vladimir V. Bakharev, Olga V. Golovina, Seminar on New Trends in Research of Energetic Materials . 2014

机译：2,4-二氨基（烷基氨基）-6-二硝基甲基-1,3,5-三嗪和2-肼基-4-氨基（烷基氨基）-6-二硝基甲基-1,3,5-三嗪的钾盐的合成
5. Synthesis and evaluation of 1,3,5-triazine derivatives of amino acids for enantiomeric resolution of amine drugs. [D] . Ayub, Muhammed. 1998

机译：氨基酸1,3,5-三嗪衍生物的合成和评估，用于胺类药物的对映体拆分。
6. Triazine-Based Tool Box for Developing Peptidic PETImaging Probes: Syntheses Microfluidic Radiolabeling and Structure–ActivityEvaluation [O] . Hairong Li, Haiying Zhou, Stephanie Krieger, -1

机译：基于三嗪的肽PET开发工具箱成像探针：合成微流体放射性标记和结构活性评价
7. Synthesis of ({8-[4,6-Bis-(bis-pyridin-2-ylmethyl-amino)-[1,3,5]triazine-2-ylamino]-octyl}—ethoxycarbonylmethyl-amino)-acetic acid ethyl ester [O] . Burkhard König, Daniel Vomasta 2007

机译：（{8- [4,6-双-（双吡啶-2-基甲基-氨基）-[1,3,5]三嗪-2-基氨基]-辛基}-乙氧基羰基甲基-氨基）-乙酸乙基的合成酯
8. Results of an acute algal study and acute oral study with 2-Amino-4-methylamino- 6-ethoxy-1,3,5-triazine, heterocycle-(triazine) with 2-Amino-4-methylamino- 6-ethoxy-1,3,5-triazine, heterocycle-(triazine) (Asterisk 1). [R] . 2011

机译：2-氨基-4-甲氨基-6-乙氧基-1,3,5-三嗪，杂环 - （三嗪）与2-氨基-4-甲氨基-6-乙氧基-1的急性藻类研究和急性口服研究结果，3,5-三嗪，杂环 - （三嗪）（asterisk 1）。

Pseudo porphyrinyl amino acids based on 1,3,5-triazine scaffold: new tools for the synthesis of peptidic porphyrins

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