Synthesis of the C9-C21 fragment of debromoaplysiatoxin and oscillatoxins A and D

Cosp A; Llacer E; Romea P; Urpi F

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Synthesis of the C9-C21 fragment of debromoaplysiatoxin and oscillatoxins A and D

机译：合成溴代海藻毒素和颤动毒素A和D的C9-C21片段

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A highly stereoselective synthesis of the C9-C21 fragment of debromoaplysiatoxin and oscillatoxins A and D has been devised. This new approach relies on the cross coupling of titanium enolates from N-acyl-1,3-thiazolidine-2-thiones and dialkyl acetals and the selective hydrogenolysis of O-benzyl protecting groups. (c) 2006 Elsevier Ltd. All rights reserved.

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2006年第32期|共5页
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Cosp A; Llacer E; Romea P; Urpi F;
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debromoaplysiatoxin; oscillatoxin; stereoselective synthesis; CHIRAL TITANIUM ENOLATE; ACETATE ALDOL REACTIONS; TUMOR PROMOTERS; ANTI-ALDOLS; APLYSIATOXIN; ACID; 30-METHYLOSCILLATOXIN-D; THIAZOLIDINETHIONES; OXAZOLIDINETHIONES; STEREOCHEMISTRIES;

机译：debromoaplysiatoxin;oscillatoxin;立体选择性合成;手性钛酸钛;乙酰乙酸酯反应;肿瘤促进剂;抗-ALDOLS;磷脂酰肌醇;酸;30-甲基螺菌毒素-D;噻唑烷二乙二烯;氧杂环丁烯酸酯;

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1. Synthesis of the C9-C21 fragment of debromoaplysiatoxin and oscillatoxins A and D [J] . Cosp A, Llacer E, Romea P, Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2006,第32期

机译：合成溴代海藻毒素和颤动毒素A和D的C9-C21片段
2. SYNTHESIS, CONFORMATION, AND BIOLOGICAL ACTIVITIES OF A DES-A-RING ANALOG OF 18-DEOXY-APLOG-1, A SIMPLIFIED ANALOG OF DEBROMOAPLYSIATOXIN [J] . Yoshiki Ashida, Ryo C. Yanagita, Yasuhiro Kawanami Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2019,第2期

机译：18-脱氧-aplog-1的DES-A环模拟的合成，构象和生物活性，德布洛斯毒素的简化类似物
3. SYNTHESIS AND BIOLOGICAL ACTIVITIES OF ACETAL ANALOGS AT POSITION 3 OF 10-METHYL-APLOG-1, A POTENTIAL ANTI-CANCER LEAD DERIVED FROM DEBROMOAPLYSIATOXIN [J] . Hayakawa Koutaro, Hanaki Yusuke, Tokuda Harukuni, Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2018,第1期

机译：缩醛类似物在10-甲基-Aplog-1的3位，衍生自Debroaaapplysiatoxin的潜在抗癌铅的合成和生物活性
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机译：1,3-二氧代-1H-茚满-2（3H）-亚烷基片段和含偶氮苯衍生物的（3-（二氰基亚甲基）-5,5-二甲基环己基-1-烯基）乙烯基片段的合成及性能
5. Development of a second-generation epoxide-based methodology for the construction of polypropionates: Application to the synthesis of the C1-C7, C8-C12, and C10-C15 polypropionate fragments of lankanolide. Stereoselective construction of all-anti polypropionate modules: Synthesis of the C5-C10 fragment of streptovaricins U and D. [D] . Rodriguez Berrios, Raul R. 2010

机译：第二代基于环氧化物的聚丙烯酸酯方法的开发：在合成兰卡醇化物的C1-C7，C8-C12和C10-C15聚丙烯酸酯片段中的应用。全抗聚丙烯酸酯模块的立体选择性构建：链霉菌素U和D的C5-C10片段的合成。
6. Natural Product Synthesis Special Feature: Synthesis of antimicrofilament marine macrolides: Synthesis and configurational assignment of a C5–C16 degradation fragment of reidispongiolide A [O] . Ian Paterson, Robert Britton, Kate Ashton, 2004

机译：天然产物合成特殊功能：抗微丝海洋大环内酯类化合物：芥子油苷A的C5–C16降解片段的合成和构型分配
7. Synthetic Studies of the 18-Membered Antitumor Macrolide, Tedanolide. 3. Stereocontrolled Synthesis of the C1-C12 Part via a Synthesis of the C1-C7 Fragment by a Mismatched but Efficient Sharpless Dihydroxylation and Its Coupling with the C8-C11 Fragment. [O] . Tomohiro MATSUSHIMA, Michiko MORI, Bao-Zhong ZHENG, 1999

机译：18元抗肿瘤大环内酯，鸡醇苷的合成研究。 3.通过不匹配但有效的无效的二羟基化的C1-C7片段合成C1-C12部分的立体控制合成，其与C8-C11片段的偶联。

Synthesis of the C9-C21 fragment of debromoaplysiatoxin and oscillatoxins A and D

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