Synthesis of pyrrolo[2,3-d]pyrimidine-2,4-diones by sunlight photolysis of N-(5-vinyluracil-6-yl)sulfilimines

Matsumoto N; Takahashi M

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Synthesis of pyrrolo[2,3-d]pyrimidine-2,4-diones by sunlight photolysis of N-(5-vinyluracil-6-yl)sulfilimines

机译：N-（5-乙烯基尿嘧啶-6-基）硫亚胺的阳光光解法合成吡咯并[2,3-d]嘧啶-2,4-二酮

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摘要

Uracil derivatives having a vinyl group at the C-5 position and a sulfilimine moiety at the C-6 position were prepared and cyclized to 1,3,6-trisubstituted pyrrolo[2,3-d]pyrimidine-2,4-diones by sunlight photolysis in good yields. (c) 2005 Elsevier Ltd. All rights reserved.

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry 》 |2005年第33期| 共4页
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Matsumoto N; Takahashi M;
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sulfilimines; uracils; sunlight; photolysis; pyrrolo2; 3-dpyrimidine-2; 4-diones; URACIL ANALOGS; SULFILIMINES; PYRROLOlt; 2; 3-Dgt; PYRIMIDINES; DERIVATIVES; PYRIDOlt; 2; 3-Dgt; PYRIMIDINES; STRATEGY; ROUTE;

机译：硫亚胺;尿嘧啶;阳光;光解;吡咯并[2;3-d]嘧啶-2;4-二酮;尿嘧啶类似物;硫化物;吡咯并2;3-D吡P酮;衍生物;吡咯并2;3-D吡MIDI;策略;路线;

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1. Synthesis of pyrrolo[2,3-d]pyrimidine-2,4-diones by sunlight photolysis of N-(5-vinyluracil-6-yl)sulfilimines [J] . Matsumoto N, Takahashi M Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2005 ,第33期

机译：N-（5-乙烯基尿嘧啶-6-基）硫亚胺的阳光光解法合成吡咯并[2,3-d]嘧啶-2,4-二酮
2. Novel Synthesis,Properties,and NAD~+-NADH Type Redox Ability of l,3-Dimethylcyclohepta[4,5]pyrrolo[2,3-d]pyrimidine-2,4(1, H)-dionylium Ions Annulated with Additional Pyrrolo[2,3-d]pyrimidine-l,3(2,4H)-dione and Furan Analogue,and Their Hydride Adduc [J] . Shin-ichi Naya, Junya Nishimura, Makoto Nitta The Journal of Organic Chemistry . 2005 ,第24期

机译：1,3-二甲基环庚[4,5]吡咯并[2,3-d]嘧啶-2,4（1，H）-重氮鎓离子与其他吡咯并合的新型合成，性质和NAD〜+ -NADH型氧化还原能力[2,3-d]嘧啶-1,3（2,4H）-二酮和呋喃类似物及其氢化物
3. Synthesis of N-{4-[(2,4-Diamino-5-methyl-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-6-yl)thio]benzoyl}-L-glutamic Acid and N-{4-[(2-Amino-4-oxo-5-methyl-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-6-yl)thio]benzoyl}-L-glutamic Acid as Dual Inhibitors of Dihyd [J] . Aleem Gangjee, Xin Lin, Roy L.Kisliuk, Journal of Medicinal Chemistry . 2005 ,第23期

机译：N- {4-[（2,4-二氨基-5-甲基-4,7-二氢-3H-吡咯并[2,3-d]嘧啶-6-基）硫代]苯甲酰基} -L-谷氨酸的合成和N- {4-[（2-氨基-4-氧代-5-甲基-4,7-二氢-3H-吡咯并[2,3-d]嘧啶-6-基）硫代]苯甲酰基} -L-谷氨酸酸作为二醛的双重抑制剂
4. Synthesis of substituted pyrrolo[2,3-d]pyrimidines as microtubule-binding agents and HSP90 inhibitors [D] . Lin, Lu 2013

机译：取代吡咯并[2,3-d]嘧啶类化合物作为微管结合剂和HSP90抑制剂的合成
5. One-pot synthesis of substituted pyrrolo34-bpyridine-45-diones based on the reaction of N-(1-(4-hydroxy-6-methyl-2-oxo-2H-pyran-3-yl)-2-oxo-2-arylethyl)acetamide with amines [O] . Valeriya G Melekhina, Andrey N Komogortsev, Boris V Lichitsky, 2019

机译：基于N-（1-（4-羟基-6-甲基-2-氧-2-氧-2H-吡喃-3-）的反应一锅合成取代的吡咯并34-b吡啶-45-二酮胺基）-2-氧代-2-芳基乙基）乙酰胺
6. Annellation of Triazole and Tetrazole Systems onto Pyrrolo[2,3-d]pyrimidines: Synthesis of Tetrazolo[1,5-c]-pyrrolo[3,2-e]-pyrimidines and Triazolo[1,5-c]pyrrolo-[3,2-e]pyrimidines as Potential Antibacterial Agents [O] . Rina D. Shah, Chaitanya G. Dave 2002

机译：将三唑和四唑体系连接到吡咯并[2,3-d]嘧啶上：四唑并[1,5-c] - 吡咯并[3,2-e] - 嘧啶和三唑并[1,5-c]吡咯并[]的合成3,2-e]嘧啶作为潜在的抗菌剂

Synthesis of pyrrolo[2,3-d]pyrimidine-2,4-diones by sunlight photolysis of N-(5-vinyluracil-6-yl)sulfilimines

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