Enantiopure hydroxylactones form D-xylose.A novel approach to the enantiodivergent synthesis of (+)-and (-)-muricatacin suitable for the preparation of 7-oxa analogues.

Velimir Popsavin; Ivana Krstic; Mirjana Popsavin

首页> 外文期刊>Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry >Enantiopure hydroxylactones form D-xylose.A novel approach to the enantiodivergent synthesis of (+)-and (-)-muricatacin suitable for the preparation of 7-oxa analogues.

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Enantiopure hydroxylactones form D-xylose.A novel approach to the enantiodivergent synthesis of (+)-and (-)-muricatacin suitable for the preparation of 7-oxa analogues.

机译：对映体纯的羟基内酯形成D-木糖。（+）-和（-）-桃红霉素的对映异构合成的新方法，适用于制备7-氧杂类似物。

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摘要

A new route towards enantiopure hydroxylactones 3 and ent-3,the final chiral precursors in an enantiodivergent synthesis of (+)- and (-)- muricatacin,has been developed starting from D-xylose.

机译：从D-木糖开始，已经开发出一种新的对映纯羟基内酯3和ent-3的途径，它们是（+）-和（-）-莫里卡星对映异构合成中的最终手性前体。

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2003年第49期|共4页
作者
Velimir Popsavin; Ivana Krstic; Mirjana Popsavin;
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5-hydroxyalkylbutan-4-olides; D-xylose; muricatacin; enantiodivergent synthesis; Wittig reaction.;

机译：5-羟烷基丁烷-4-内酯;D-木糖;多卡他霉素;对映异构合成;Wittig反应。;

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1. Enantiopure hydroxylactones form D-xylose.A novel approach to the enantiodivergent synthesis of (+)-and (-)-muricatacin suitable for the preparation of 7-oxa analogues. [J] . Velimir Popsavin, Ivana Krstic, Mirjana Popsavin Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2003,第49期

机译：对映体纯的羟基内酯形成D-木糖。（+）-和（-）-桃红霉素的对映异构合成的新方法，适用于制备7-氧杂类似物。
2. ENANTIOPURE HYDROXYLACTONES FROM L-ASCORBIC AND D-ISOASCORBIC ACIDS .1. SYNTHESIS OF (-)-MURICATACIN [J] . Saniere M., Lemerrer Y., Depezay JC., Tetrahedron . 1995,第6期

机译：L-抗坏血酸和D-异抗坏血酸的对映体羟基内酯.1。（-）-番木瓜素的合成
3. A convenient chiron approach to (4R,5R)-5-hydroxyalkylbutan-4-olides and the corresponding 7-oxa analogues from D-(+)-mannitol via an advanced common precursor: syntheses of (-)-muricatacin, 7-oxa-(-)-muricatacin, (4R,5R)-(-)-5-hydroxy-4-decanolide, and (4R,5R)-(-)-7-oxa-5-hydroxy-4-dodecanolide [J] . Chatterjee Sandip, Manna Avrajit, Bhaumik Tanurima Tetrahedron, Asymmetry: The International Journal for Repid Publication on all Aspects of Asymmetry in Orgainc, Inorganic, Organometallic, Physical and Bio-Organic Chemistry . 2014,第24期

机译：通过先进的常见前体从D-（+）-甘露糖醇制取（4R，5R）-5-羟烷基丁烷-4-油化物和相应的7-oxa类似物的简便的卡隆方法：（-）-多卡他霉素，7-oxa的合成-（-）-多卡他霉素，（4R，5R）-（-）-5-羟基-4-癸醇化物和（4R，5R）-（-）-7-氧杂-5-羟基-4-十二烷醇化物
4. Novel approach for enantiopure azapeptide synthesis:application of N-Boc-aza-dipeptides in solution-and solid-phase peptide chemistry [C] . Rosa E.Melendez, William D.Lubell European Peptide Symposium . 2002

机译：对脱氮氮化物合成的新方法：在溶液与固相肽化学中的N-Boc-Aza-Dipeptics应用
5. I. Synthesis of new thio- and selenoglycosides towards glycomimetics and enzyme inhibition. II. Preparations and reactions of thio- and selenocarboxylates. III. Synthesis of mycothiol analogues. [D] . Darout, Etzer. 2005

机译：I.针对糖模拟物和酶抑制的新的硫代和硒代糖苷的合成。二。硫代和硒代羧酸盐的制备和反应。三，麦硫酚类似物的合成。
6. A Short Synthesis of Aphanamol I in Both Racemic and Enantiopure Forms [O] . Dr. Steven J. Ferrara, Dr. Jonathan W. Burton -1

机译：外消旋和对映体纯形式的Aphanamol I的快速合成
7. An approach towards chiral 5-hydroxyalkyl butan-4-olides: total synthesis of (-)-muricatacin and related natural products [O] . M. Chandrasekhar, Kusum L. Chandra, Vinod K. Singh 2002

机译：手性5-羟烷基丁-4-醇的方法：（ - ） - muricatacin及相关天然产物的全合成

Enantiopure hydroxylactones form D-xylose.A novel approach to the enantiodivergent synthesis of (+)-and (-)-muricatacin suitable for the preparation of 7-oxa analogues.

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