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首页> 外文期刊>Journal of chromatography, A: Including electrophoresis and other separation methods >Novel multi-gas chromatography-olfactometry device and software for the identification of odour-active compounds
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Novel multi-gas chromatography-olfactometry device and software for the identification of odour-active compounds

机译:用于气味活性化合物鉴定的新型多气相色谱-嗅觉测定仪和软件

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The aim of this work was to devise a novel fully computerised chromatography-olfactometry system where eight sniffers detect volatile compounds obtained from a single chromatographic separation. The technical options taken to implement this system are described in detail. The new methods and software developed and applied to analyse data obtained by gas chromatography-olfactometry and mass spectrometry (GC-O/MS) are presented. We found that 46 odorous zones could be detected by a panel of eight sniffers during the 35 min of the analysis of the volatile compounds extracted from a cheese by purge-and-trap. Synchronisation of olfactometry and mass spectrometry data enabled us to propose 44 structures to account for 44 out of these 46 odorous zones. (c) 2007 Elsevier B.V. All rights reserved.
机译:这项工作的目的是设计一种新颖的,完全计算机化的色谱-嗅觉测定系统,其中八个嗅探器可检测从一次色谱分离中获得的挥发性化合物。详细介绍了用于实施此系统的技术选项。介绍了开发和应用的新方法和软件,用于分析通过气相色谱-嗅觉和质谱(GC-O / MS)获得的数据。我们发现,在35分钟内,通过吹扫捕集法从奶酪中提取的挥发性化合物的分析过程中,由八个嗅探器组成的面板可以检测到46个气味区域。嗅觉和质谱数据的同步使我们能够提出44种结构,以解释这46个臭味区中的44个。 (c)2007 Elsevier B.V.保留所有权利。

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