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Relative intensities of different reflection order X-ray lines registered by microprobe analyzers

机译:微探针分析仪记录的不同反射阶数X射线线的相对强度

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Relative intensities of X-ray lines for various reflection orders are measured using a JXA-8100 microprobe analyzer. Spectra obtained using standard analyzing crystals LiF, PET, TAP, LDE1, and LDE2 are studied. We observe and explain specific features of spectrometers with curved analyzing crystals that influence higher order reflections. The second-order intensities are similar for different analyzing crystals and lie in the range 2.4 (PET)-5.6% (LiF) of the first-order intensity. Higher order reflections show more variation. For example, for the LDE2 crystal, no lines of higher than the second-order were observed, whereas for TAP reflections of up to eighth order were detected. The data obtained may be used for reference purposes.
机译:使用JXA-8100微型探针分析仪测量各种反射阶数的X射线线的相对强度。研究了使用标准分析晶体LiF,PET,TAP,LDE1和LDE2获得的光谱。我们观察和解释具有弯曲分析晶体的光谱仪的特定功能,这些晶体会影响高阶反射。不同分析晶体的二阶强度相似,处于一阶强度的2.4(PET)-5.6%(LiF)范围内。高阶反射显示更多变化。例如,对于LDE2晶体,没有观察到高于第二阶的线,而对于TAP反射,检测到高达八阶。获得的数据可用于参考目的。

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