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Characteristic and magnetic properties of Ni1-xZnxFe2O4 ferrites

机译:Ni1-xZnxFe2O4铁氧体的特性和磁性

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Ferrites are magnetic ceramic materials which have additional metallic ion in ferrous oxide compounds. Ferrites are usually classified as soft or hard ferrites. In this study, characteristics and magnetic properties of magnetic materials having NiO1-xZnOxFe2O4 structure were investigated. Mechanical mixing of high purity NiO, ZnO and Fe2O3 powders were done to obtain homogenous NiO1-xZnOxFe2O4 powder mixture for x = 0.15, x = 0.50 and x = 0.85. These powder mixtures were pressed using hydraulic press machine and then subjected to sintering at same temperatures of 1000 degrees C for 1 hour. Obtained specimens were analyzed with scanning electron microscopy (SEM) imaging and energy dispersive X-ray fluorescence (EDXRF) technique for the investigation of structural analysis; magnetic properties were determined using vibrating sample magnetometer (VSM). However, effects of composition, specimens and Zn% element in magnetic materials after energy dispersive X-ray fluorescence on maximum magnetic moment (M-s) were analyzed using Taguchi orthogonal array design of experiments technique. The study indicates that Zn% element is the main process parameter that has the highest statistical influence on maximum magnetic moment. However, another parameter, composition, also has a significant effect on maximum magnetic moment. Then, Zn-content was found to have a significant influence on the magnetic properties of the system.
机译:铁氧体是磁性陶瓷材料,在氧化亚铁化合物中具有额外的金属离子。铁氧体通常被分类为软或硬铁氧体。在这项研究中,研究了具有NiO1-xZnOxFe2O4结构的磁性材料的特性和磁性能。机械混合高纯度的NiO,ZnO和Fe2O3粉末以获得x = 0.15,x = 0.50和x = 0.85的均匀NiO1-xZnOxFe2O4粉末混合物。使用液压机将这些粉末混合物压制,然后在相同的1000℃温度下烧结1小时。用扫描电子显微镜(SEM)成像和能量色散X射线荧光(EDXRF)技术对获得的标本进行分析,以研究结构分析;使用振动样品磁力计(VSM)确定磁性。然而,使用田口正交实验设计,分析了能量色散X射线荧光后磁性材料中的成分,标本和Zn%元素对最大磁矩(M-s)的影响。研究表明,Zn%元素是对最大磁矩具有最大统计影响的主要工艺参数。但是,另一个参数(成分)也对最大磁矩有重大影响。然后,发现锌含量对系统的磁性能有重大影响。

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