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Mechanical extraction of shea butter: Optimisation and characterisation studies with comparison to other methods of extraction

机译:乳木果油的机械提取:与其他提取方法相比,优化和表征研究

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Shea butter (SB) production by mechanical extraction (ME) was optimised by box-behnken (BB) experimental designof response surface methodology (RSM). The process parameters studied (with their ranges) were sample weight (100 – 200 g),temperature (60 – 120oC) and duration of applied pressure (10 – 30 min) to optimise the yield of SB. The characteristics of theSB were determined using standard methods and Fourier transform infrared spectroscopy (FTIR). A comparative study of the SBfrom ME with other methods of extraction was also performed. The optimum 37% (w/w) yield of SB was obtained from 150 gsample of shea kernel at 90oC and 20 min. The R2 (0.9957) obtained from analysis of variance showed that quadratic model ofBB fitted the experimental data well. The characteristics of the SB from ME showed non-compromising quality, with a yieldgreater than that of traditional method but lower than with solvent method. This study showed that the extraction methods affectboth yield and quality of SB.
机译:通过Box-behnken(BB)响应面方法(RSM)的实验设计,优化了通过机械萃取(ME)生产的乳木果油(SB)。研究的工艺参数(及其范围)为样品重量(100 – 200 g),温度(60 – 120oC)和施加压力的持续时间(10 – 30分钟),以优化SB的收率。使用标准方法和傅里叶变换红外光谱(FTIR)确定了SB的特性。还进行了来自ME的SB与其他提取方法的比较研究。在90oC和20分钟下从150 g乳木果样品中获得SB的最佳37%(w / w)收率。通过方差分析获得的R2(0.9957)表明BB的二次模型很好地拟合了实验数据。 ME的SB的特性显示出不妥协的质量,收率比传统方法高,但低于溶剂法。研究表明,提取方法对SB的产量和品质都有影响。

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